Medicine for treating diabetes and production method thereof
A technology for diabetes drugs and production methods, applied in drug combinations, medical formulas, metabolic diseases, etc., can solve the problems of lack of scientific quality standards, difficulty in determining active ingredients, lack of modernization of traditional Chinese medicine, etc., to achieve rich drug sources and simplified prescriptions , the effect of treating and preventing diabetes
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Embodiment 11
[0029] The extraction of embodiment 1.1 corn silk total saponins:
[0030] Weigh the dry product of Chinese herbal corn silk to make regular decoction pieces, use 10-14 times the amount of 60-95% ethanol to reflux extract 2-3 times; or decoct the extract with water, decoct 3 times with 10-12 times the amount , one hour each time, the extract is precipitated with 60-95% ethanol, the supernatant is decolorized with 2% medicinal activated carbon, filtered, and the ethanol is recovered until there is no alcohol smell, then extracted 2-3 times with water-saturated n-butanol, and the Recover n-butanol under pressure, and dry the concentrate to obtain total saponins from corn silk. Take a small amount of total saponins, and use Libermann-Burcherd color reaction to carry out identification test: a purple-red reaction occurs between chloroform and the color developer, indicating that the substance is a triterpene saponin. Visible-ultraviolet spectrophotometer was used to measure ginse...
Embodiment 12
[0031] The alcohol extraction method of embodiment 1.2 corn silk total saponins is extracted:
[0032] Choose fresh dry corn silk, process and cut it, 3-5cm long, use 70% ethanol, the ratio of solid to liquid is 1:12, soak for 2 hours, put it into the extraction cylinder of Soxhlet extractor, and reflux extraction twice, For 1.5 hours each time, combine two alcohol extracts, high-speed centrifugation, 3000-3500r / min, 15', take the supernatant, distill under reduced pressure, recover ethanol, the specific gravity of the concentrated solution is 1.10-1.25g / cm at 50°C 3 , and then extracted with water-saturated n-butanol, a total of 3 extractions, collected the n-butanol layer, distilled under reduced pressure, recovered n-butanol, and placed the concentrated solution in a vacuum drying oven at a temperature of 60°C and a vacuum pressure of 0.08-0.1mpa , and vacuum-dried to obtain a dry thick paste, which is the total saponins of corn silk.
[0033] Select the four factors of et...
Embodiment 13
[0034] The alcohol extraction method of embodiment 1.3 corn silk total saponins is extracted:
[0035] Choose fresh dried corn silk, after cutting, weigh 250kg, put it into a multi-functional extraction tank, use 70% ethanol, which is 11-12 times the weight of the medicinal material, soak for 2 hours, and carry out reflux extraction at a temperature of 50°C in the tank , a total of 2 extractions, each time 2h. The ethanol extract is concentrated by an external heating circulation concentrator, the ethanol is recovered, and concentrated to a specific gravity of 1.08-1.15g / cm at 50°C 3 , extracted with water-saturated n-butanol, extracted twice, n-butanol extract was distilled under reduced pressure, n-butanol was recovered, the concentrated solution was put into a vacuum desiccator, the vacuum pressure was 0.08-0.09mpa, the temperature was 60°C, and dried. The yellowish-brown powdery dry product is the total saponins of corn silk. The method is especially suitable for industr...
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