Preparation method of polypropylene millipore filtration sheet material
A technology of microporous filtration and polypropylene, which is applied in the direction of flat products, applications, household appliances, etc., can solve the problem that it is difficult to meet the requirements of polypropylene microporous filter pore density and gas transmission rate, and the micropores are easy to form closed micropores , High production cost and other issues, to achieve the effect of controlling air permeability and pressure bearing performance, low production cost, and short production cycle
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Embodiment 1
[0037] (1) Add 85 parts of homopolypropylene powder with a particle size of 10 to 150um and a melt flow rate (MFR) of 1.0g / 10min and 7 parts of n-octane into a high-speed mixer, at 1400 rpm Stir and mix at a rotating speed until the temperature rises to 80°C, stop stirring, and cool to obtain polypropylene powder containing a low-boiling liquid foaming agent;
[0038] (2) Add 2.5 parts of azodicarbonamide, 2.0 parts of polyoxypropylene stearate, 1.5 parts of calcium stearate, 0.5 parts of stearic acid, 0.48 parts of sodium benzoate, and 1.0 parts of liquid paraffin into a three-roll mill (or ball mill) for 5 minutes to form a uniform and fine paste;
[0039] (3) Add the obtained paste to a high-speed mixer equipped with polypropylene powder containing a low-boiling liquid foaming agent, and continue to stir and mix for 5 minutes at a speed of 1400 rpm to make the paste Evenly adhere to the surface of polypropylene powder containing low boiling point liquid foaming agent;
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Embodiment 2
[0043] (1) 45 parts of homopolypropylene powder with particle size of 10-150um and MFR of 1.0g / 10min, 41 parts of homopolypropylene powder with particle size of 10-150um and MFR of 6.5g / 10min, Add 5.0 parts of n-pentane and 3.0 parts of Vaseline into a high-speed mixer, stir and mix at a speed of 1800 rpm until the temperature rises to 70°C, stop stirring, and cool to obtain polypropylene powder containing a low-boiling point liquid foaming agent material;
[0044] (2) 2.0 parts of potassium azocarboxamide formate, 0.5 parts of fatty alcohol polyoxyethylene ether, 1.5 parts of urea, 1.0 parts of stearic acid, 0.02 parts of dicumyl peroxide, 1.0 parts of maleic anhydride, 0.5 parts of liquid paraffin Add the three-roller mill (or ball mill) and grind for 10 minutes to form a uniform and fine paste;
[0045] (3) Add the obtained paste to a high-speed mixer equipped with polypropylene powder containing a low-boiling liquid foaming agent, and continue to stir and mix for 5 minute...
Embodiment 3
[0049] (1) Add 80 parts of homopolypropylene powder with a particle size of 100-200um and an MFR of 2.5g / 10min and 10 parts of n-decane into a high-speed mixer, and stir at a speed of 1800-2000 rpm Mix until the temperature rises to 75-90°C, stop stirring, and cool down to obtain polypropylene powder containing low-boiling liquid foaming agent;
[0050] (2) 2.0 parts of N, N'-dinitropentamethylenetetramine, 2.0 parts of fatty alcohol polyoxyethylene ether, 1.5 parts of zinc stearate, and 2.0 parts of superfine calcium carbonate with a particle size of 1 to 100um, 0.48 parts of potassium hydrogen terephthalate, 0.02 parts of 2,5-dimethyl-2,5-bis(tert-butylperoxy)hexane, 1.0 parts of maleimide, 2.5 parts of methylphenyl silicone oil Together, add it to a three-roller mill (or ball mill) and grind for 15 minutes to form a uniform and fine paste;
[0051] (3) Add the obtained paste to a high-speed mixer equipped with polypropylene powder containing a low-boiling liquid foaming ag...
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