Cathode catalyst for fuel cell, membrane-electrode assembly for fuel cell comprising same and fuel cell system comprising same
A technology of fuel cell system and cathode catalyst, which is used in fuel cell parts, fuel cells, battery electrodes, etc.
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Embodiment 1
[0074] By mixing 1 g of Ru(CH 3 COO) 3 , 0.5g of W(CH 3 COO) 3 , 15 g CH 3 CSNH 2 , and 12ml of Triton X-100, and stirred with a magnetic stirring bar for 15 minutes to prepare the first emulsion.
[0075] By mixing 16 g of C in a flask 6 h 12 (cyclohexane), and 8ml of Triton X-100, and stirred with a magnetic stirring bar for 15 minutes to prepare the second emulsion.
[0076] The prepared first and second emulsions were added to the flask and mixed by swirling the magnetic stir bar therein for 15 minutes. The flask containing the mixture of the first and second emulsions was then heated to 60°C and maintained at 60°C for 8 hours, then cooled to room temperature. Next, the mixture in the flask was filtered to obtain a precipitate. The precipitate was washed three times with distilled water and ethanol, and dried at 60° C. for 4 hours to obtain nanowire-shaped Ru-W-S. The Ru-W-S contains 54 atomic % of Ru, 24 atomic % of W, and 22 atomic % of S, and has 100m 2 / g sp...
Embodiment 2
[0079] By mixing 1.6 g of H in the flask 2 RhCl 4 , 0.9g of Mo(CO) 6 , 15 g CH 3 CSNH 2 , and 12ml of Triton X-100, and stirred for 15 minutes with a magnetic stirring bar to prepare the first emulsion.
[0080] By mixing 16 g of C in a flask 6 h 12 (cyclohexane), and 8ml of Triton X-100, and stirred with a magnetic stirring bar for 15 minutes to prepare the second emulsion.
[0081] The prepared first and second emulsions were added to the flask and stirred with a magnetic stir bar therein for 15 minutes to effect mixing. The flask containing the first and second emulsion mixtures was then heated to 60°C and held at 60°C for 8 hours, then cooled to room temperature. Next, the mixture in the flask was filtered to obtain a precipitate. The precipitate was washed 3 times with distilled water and ethanol, and dried at 60°C for 4 hours to obtain nanowire-shaped Rh-Mo-S. The Rh-Mo-S contains 67 atomic percent Rh, 23 atomic percent Mo, and 10 atomic percent S, and has 110m ...
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