Naphthalenedione compounds
A compound, C1-C6 technology, applied in the direction of active ingredients of hydroxyl compounds, active ingredients of heavy metal compounds, drug combinations, etc., can solve problems such as poor results, side effects, and unsatisfactory
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Embodiment 1
[0065] Some compounds were isolated from Amebia euchroma (Royle) Johnst. Specifically, 1.65 kg of medicinal materials were soaked in 32 L of acetone for 3 days, and then filtered through a 200 mesh filter. The filtrate was concentrated under vacuum to obtain herbal extracts. 100 mg of the extract was dissolved in 50 ml of 100% methanol. The solution was sonicated for 30 minutes and filtered through a 0.45 micron filter membrane. It was processed by HPLC and eluted with 75% methanol. Six compounds were detected and separated by HPLC. The chromatographic conditions of analytical HPLC are: mobile phase: (A)H 2 O: CH 3 CN: AcOH = 800 ml: 200 ml: 10 ml, (B) H 2 O: CH 3 CN: MeOH: AcOH = 100 ml: 450 ml: 450 ml: 1 ml; flow rate, 0.8 ml / min; detection wavelength, 515 nm: column temperature, 40°C; gradient, linear from 10% B to 100% B; run Time, 60 minutes.
[0066]Collect fractions containing each compound. Under vacuum, the solvent in the collected fraction was removed to obtain a residue...
Embodiment 2
[0070] Using Carter's equivalent in 1991 in J. Pharmacol. Exp. Ther., 256(3): 929-937 and Safayhi's equivalent in 2000 in Planta Medica, 66: 110-113 and the modified method to study the above compounds (1 or 10μM) and the effect of extracts prepared from Xinjiang Lithospermum on 5-lipoxygenase activity. They were found to inhibit 5-lipoxygenase activity. Use nordihydroguaiaretic acid (NDGA), epigallocatechin-3 gallate (EGCG) and ciclpirox olamine as positive controls. The results are summarized below Table 2A and 2B.
[0071] Table 2A Inhibition of 5-lipoxygenase I
[0072]
[0073] Table 2B 5-Lipoxygenase II Inhibition
[0074]
[0075] It is known that 5-lipoxygenase is a key enzyme in the biosynthesis of leukotrienes and an important mediator in the process of inflammation and allergy. This result suggests that these compounds have dual anti-inflammatory and anti-allergic activities. The experiment was repeated with different concentrations of compounds, and similar results...
Embodiment 3
[0077] The activity of the above-mentioned compounds and extracts on Acne bacillus (a bacterial agent that causes pimples (acne)) was studied. Specifically, using Modugno equal to 1994 in Antimicrobial Agents and Chemotherapy, 38:2362-2368 and Missiek equal to 1973 in Antimicrobial Agents Chemtherapy, 3:40-48, the modified method was used to examine the compound or extract against bacteria (ATCC6919) Inhibition of growth. The results are summarized in Table 3.
[0078] Table 3 Anti-acne bacillus activity
[0079]
[0080] The results indicate that the above compounds and extracts can be used to treat acne infections.
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