Quaternized Cellulose Ethers for Personal Care Products
A personal care, cellulose ether technology, applied in skin care preparations, hair care, cosmetic preparations, etc., can solve the problems of reduced foaming, poor viscosity maintenance, poor thickening efficiency, etc.
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Embodiment 1
[0032] The quaternized cellulose ethers of the present invention are obtained in combination with the various components listed in Table 1 below:
[0033] Table 1
[0034]
batch 1
batch 2
batch 3
(Compared)
batch 4
batch 5
(Compared)
batch 6
batch 7
HEC 1
60
--
--
--
--
--
--
HEC 2
--
80
40
--
300
40 *
80
HEC 3
--
--
--
60
--
--
--
360
480
240
--
--
--
460
6% isopropyl alcohol (IPA) in water
--
--
--
--
1805
--
--
0% IPA in water
--
--
--
--
--
241
--
2% IPA in water
--
--
--
360
--
--
--
25% by weight sodium hydroxide (NaOH)
...
Embodiment 2
[0044] Following essentially the protocol of Example 1, the batches listed in Table 1 were prepared and characterized. The results are listed in Table 2:
[0045] Table 2
[0046]
[0047]Compounds of batches 1-7 may be represented by formula (II) above, wherein n is about 500-2000, x is selected such that the hydroxyethyl substitution M.S. is about 2.0 to 2.4, and y and z are selected such that the batch Subcompounds have the nitrogen percentages and levels of hydrophobic substitution (HS) listed in Table 2. Nitrogen content, %N: average weight percentage of nitrogen per anhydroglucose repeating unit determined by titration using an automated Buchi Kieldahl distillation unit and by an automated titrimeter. The average number of moles of hydrophobic substituents per mole of anhydroglucose units is expressed as hydrophobic substitution (HS). Using nuclear magnetic resonance ( 1 H-NMR, 400 MHz, using sodium trimethylsilyl propionate as a standard and heavy water as...
Embodiment 3
[0049] The personal care composition of the present invention comprises the quaternized cellulose ether from Example 1 with the components listed in Table 3:
[0050] table 3
[0051] Batch A
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