Small RNA and application thereof
A technology of tiny nucleic acids and oligonucleotides, applied in the field of biomedical materials, can solve the problems of lack of diagnostic sensitivity and repeatability of patients, and achieve the effect of convenient sampling
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Embodiment 1
[0040] The preparation of embodiment 1 total RNA
[0041] A: Isolation of peripheral blood mononuclear cells (PBMCs)
[0042] (1). Collect blood with an anticoagulant tube (containing 0.2ml of anticoagulant solution), shake well, and add Hank's solution or PBS equal volume (1:1) to dilute the blood.
[0043] (2). Take 2ml of lymphocyte stratification solution and put it into a 15ml centrifuge tube.
[0044] (3). Tilt the centrifuge tube at an angle of 45°, absorb the diluted blood with a straw, and add it slowly along the wall of the test tube at a distance of 1cm from the layered liquid surface, so that the diluted blood is stacked on the layered liquid, and the interface between the two is kept clear. . (The volume ratio of diluted blood to layered fluid is about 2:1).
[0045] (4). Centrifuge in a horizontal centrifuge at 2000rpm for 20min at 18-20°C. After centrifugation, the contents are divided into four layers. The upper layer is plasma (containing platelets), the mi...
Embodiment 2
[0059] Example 2 Gene chip analysis microRNA expression profile (gene chip purchased from Invitrogen)
[0060] (1). Extraction of peripheral blood mononuclear cells, total RNA and miRNA
[0061] Extract 10 specimens of active AS patients before treatment, 10 specimens of AS patients after 12 weeks of Enbrel treatment, and 10 specimens of healthy controls with 4ml of venous blood, and extract PBMCs by the method described in Example 1. Total RNA was extracted with TRIzolReagent (Life Technologies, Inc.), and miRNA was isolated with mirVana microRNAIsolation Kit (Ambion, Inc.), and stored at -20°C.
[0062] (2). miRNA chip labeling and purification
[0063]Vacuum-dry 2--5 μg of microRNA. After drying, resuspend the microRNA sample with 4 μl Nuclease-freeWater; use mirVana TM microRNA Labeling Kit (Ambion Inc.) with Monoreactive Cy3 dye / Monoreactive Cy5dye (Amersham Pharmacia Biotech, Ltd) as fluorescent label , QIAgene PCR Purification kit (QIAGEN, Inc.); the next step of puri...
Embodiment 3
[0068] Preparation of embodiment 3cDNA (total RNA reverse transcription):
[0069] The total RNA extracted in Example 1 was reverse-transcribed to prepare a cDNA template (reverse transcription primer sequences are shown in Table 1).
[0070] A: Reverse transcription reaction system:
[0071] Reagent name (both buffer and enzyme are
promega company)
Dosage / tube
5×Reverse Transcription buffer
(buffer)
4ul
RT Primer Mix (1uM) (primer mixture)
1.25ul
dNTP (10mM) (four deoxyribonucleotides
Mixture)
0.75ul
RNA (template)
2ul
RTase (200U / ul) (reverse transcriptase)
0.5ul
DEPC H2O
to 20ul
[0072] B: Reverse transcription reaction conditions:
[0073] The reaction conditions are: 16°C for 30 minutes; 42°C for 30 minutes; 85°C for 10 minutes.
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