Extraction method of ginseng, ophiopogon root and shiandra and preparation thereof
A technology of schisandra and ginseng, applied in the field of Yiqi Fumai preparation for treating cardiovascular diseases and its preparation, achieving the effects of low cost, less dosage, and easy long-term storage
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Embodiment 1
[0076] (1) Ginseng fibrous root coarse powder, ginseng slices, crushed into granules;
[0077] (2) Add 8 times the amount of water-containing lower alcohol, the concentration of water-containing lower alcohol is 60%, reflux extraction 6 times, each time for 3 hours, the lower alcohol is ethanol;
[0078] (3) degreasing with dichloromethane, extracting with n-butanol, concentrating the extract, merging the extract, concentrating the extract to obtain a medicinal extract, and obtaining a single extract of ginseng;
[0079] (2) Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0080] (1) Ophiopogon japonicus, crushed into granules;
[0081] (2) 90% ethanol percolation, the amount of ethanol is 18 times, the time is 24 hours, degreasing;
[0082] (3) Ophiopogon japonicus is dried to remove alcohol after percolation;
[0083] (4) Add 8 times the amount of water, extract 3 times at 90°C, 1 hour each time;
[0084] (5) Filtrate while hot, ad...
Embodiment 2
[0098] (1) Ginseng fibrous root coarse powder, ginseng slices, crushed into granules;
[0099] (2) Add 8 times the amount of water-containing lower alcohol, the concentration of water-containing lower alcohol is 60%; reflux extraction 6 times, each time for 3 hours, the lower alcohol is ethanol;
[0100] (3) degreasing with dichloromethane, extracting with n-butanol, concentrating the extract, combining the extract, concentrating the extract to obtain a medicinal extract, and obtaining a single extract of ginseng;
[0101] (2) Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0102] (1) Ophiopogon japonicus, crushed into granules;
[0103] (2) 90% ethanol percolation, the amount of ethanol is 18 times, the time is 24 hours, degreasing;
[0104] (3) Ophiopogon japonicus is dried to remove alcohol after percolation;
[0105] (4) Add 8 times the amount of water, extract 3 times at 90°C, 1 hour each time;
[0106] (5) Filtrate while hot, ...
Embodiment 3
[0120] (1) Ginseng fibrous root coarse powder, ginseng slices, crushed into granules;
[0121] (2) Add 6 times the amount of water-containing lower alcohol, the concentration of water-containing lower alcohol is 45%, reflux extraction 2 times, each time for 0.5 hours, the lower alcohol is methanol;
[0122] (3) Combine the extracts, concentrate the extracts to obtain extracts, and obtain the product as a single extract of ginseng;
[0123] (2) Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0124] (1) Ophiopogon japonicus, crushed into granules;
[0125] (2) 85% ethanol percolation, the amount of ethanol is 12, the time is 128 hours, degreasing;
[0126] (3) Ophiopogon japonicus is dried to remove alcohol after percolation;
[0127] (4) Add 6 times the amount of water, extract 2 times at 85°C, 0.5 hours each time;
[0128] (5) Filtrate while hot, add 0.2% activated carbon to the extract to decolorize for 2 hours, at room temperature...
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