Preparation method of gardenia green pigment
A gardenia green and pigment technology, applied in chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problems of difficult control, large differences between product batches, etc., and achieves low cost, good stability, and technology. Simple and easy to control effects
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Embodiment 1
[0028] Take 1kg of dried gardenia fruit, crush it, put it into a container, add 5kg of water, and add 50g of cellulase, control the temperature at 45°C, the pH of the system is 5, extract for 4 hours, and stir at a speed of 50r / min; after the extraction, Remove the residue by centrifugation, and collect the extract; add 0.3kg of sodium glutamate to the extract, react at 50°C for 48 hours, and stir at a speed of 80r / min; after the reaction, filter the reaction solution to remove insoluble impurities. The gardenia green pigment solution is obtained; the gardenia green pigment solution is dehydrated and dried, and the obtained dry powder is the prepared gardenia green pigment.
Embodiment 2
[0030] Take 1 kg of dried gardenia fruit, crush it, put it into a container, add 8 kg of water, and add 20 g of β-glucosidase, control the temperature at 50 ° C, the pH of the system is 6, extract for 3 hours, and the stirring speed is 100 r / min; the extraction is completed Afterwards, the residue was removed by filtration, and the extract was collected; 0.5kg of phenylalanine was added to the extract, and reacted at 55°C for 36h, with a stirring speed of 120r / min; after the reaction, the reaction solution was filtered to remove the insoluble impurities to obtain a gardenia green pigment solution; the gardenia green pigment solution is dehydrated and dried, and the obtained dry powder is the prepared gardenia green pigment.
Embodiment 3
[0032] Take 1t of dried gardenia fruit, crush it, put it into a container, add 5t of water, and add 10kg of pectinase. , after filtering, the extract was collected, and the filter residue was added to 3t water for the second extraction, the extraction conditions were the same as the first time, after the end, filtered, and the extract was combined; 0.2t glutamic acid was added to the extract, and the React at 50°C for 60 hours, with a stirring speed of 120r / min; after the reaction, filter the reaction solution to remove insoluble impurities to obtain a gardenia green pigment solution; dehydrate and dry the gardenia green pigment solution to obtain a dry powder That is the prepared gardenia green pigment.
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