Printing ink cleaning solvent and preparation method thereof
A solvent and printing ink technology, applied in the field of ink cleaning solvent and its preparation, can solve problems such as adverse effects on human health, reduced service life, surface cracks, etc., and achieve the effects of improving cleaning efficiency, saving resources, and reducing volatilization
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Embodiment 1
[0043] 1. The recovered natural oil is filtered, dried and precipitated, and then heated to 80°C to become a liquid1;
[0044] 2. Prepare sulfuric acid and methanol into agent A in a weight ratio of 1:30;
[0045] 3. Add agent A into liquid 1 at a volume ratio of 1:8, control the temperature at 80°C, stir and react for 1 hour to form agent B;
[0046] 4. After agent B is left to stand for 12 hours, the bottom color light brown solution F1 will be released, and the rest will become liquid 2.
[0047] 5. Prepare caustic soda and methanol according to the weight ratio of 1:30 to form C agent;
[0048] 6. Heat liquid 2 to 80°C, add agent C to liquid 2 at a volume ratio of 1:6, stir and mix for 1 hour, keep warm for 3.5 hours, and release bottom solution F2.
[0049] 7. Draw out and condense the methanol under negative pressure. During this process, continue to stir and keep the temperature for 45 minutes, then cool down naturally.
[0050] 8. After standing still for 12 hours, ...
Embodiment 2
[0055] 1. Natural oil is heated to 75°C to become liquid 1;
[0056] 2. Prepare sulfuric acid and methanol into agent A in a weight ratio of 1:25;
[0057] 3. Add agent A into liquid 1 at a volume ratio of 1:6, control the temperature at 75°C, stir and react for 2 hours to form agent B;
[0058] 4. After agent B is left to stand for 13 hours, the bottom color light brown solution F1 will be released, and the rest will become liquid 2.
[0059] 5. Prepare caustic soda and methanol according to the weight ratio of 1:25 to form C agent;
[0060] 6. Heat the liquid 2 to 75°C, add agent C to the liquid 2 at a volume ratio of 1:8, stir and mix for 2 hours, keep it warm for 3 hours, and release the bottom solution F2.
[0061] 7. Draw out and condense the methanol under negative pressure. During this process, continue to stir and keep the temperature for 60 minutes, then cool down naturally.
[0062] 8. After standing still for 13 hours, release the bottom layer solution F3 (light...
Embodiment 3
[0067] 1. The recovered natural oil is filtered, dried and precipitated, and then heated to 85°C to become a liquid1;
[0068] 2. Prepare sulfuric acid and methanol into agent A in a weight ratio of 1:35;
[0069] 3. Add agent A into liquid 1 at a volume ratio of 1:10, control the temperature at 85°C, stir and react for 0.5 hours to form agent B;
[0070] 4. After agent B is left to stand for 12 hours, the bottom color light brown solution F1 will be released, and the rest will become liquid 2.
[0071] 5. Prepare caustic soda and methanol according to the weight ratio of 1:35 to form C agent;
[0072] 6. Heat the liquid 2 to 85°C, add agent C to the liquid 2 at a volume ratio of 1:10, stir and mix for 0.5 hours, keep it warm for 4 hours, and release the bottom solution F2.
[0073] 7. Draw out and condense the methanol under negative pressure. During this process, continue to stir and keep the temperature for 30 minutes, then cool down naturally.
[0074] 8. After standing s...
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