Printing ink cleaning solvent and preparation method thereof
A solvent and printing ink technology, applied in the field of ink cleaning solvent and its preparation, can solve problems such as adverse effects on human health, shortening service life, and burning, and achieve the effects of improving cleaning efficiency, saving resources, and reducing waste.
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Embodiment 1
[0043] 1. The recovered natural oil is filtered, dried and precipitated and heated to 80℃ to become liquid 1;
[0044] 2. Formulate sulfuric acid and methanol into A agent according to the weight ratio of 1:30;
[0045] 3. Add agent A to liquid 1 at a volume ratio of 1:8, control the temperature at 80°C, stir and react for 1 hour to form agent B;
[0046] 4. After agent B is allowed to stand for 12 hours, the bottom color light brownish yellow solution F1 is released, and the rest becomes liquid 2.
[0047] 5. Prepare caustic soda and methanol at a weight ratio of 1:30 to form agent C;
[0048] 6. Heat liquid 2 to 80°C, add agent C to liquid 2 in a volume ratio of 1:6, stir and mix for 1 hour, keep it for 3.5 hours, and release the bottom layer solution F2.
[0049] 7. Extract and condense the methanol under negative pressure, continue to stir and keep the temperature for 45 minutes during this process, then cool down naturally.
[0050] 8. After standing for 12 hours, the bottom layer so...
Embodiment 2
[0055] 1. The natural oil is heated to 75℃ to become liquid 1;
[0056] 2. Formulate sulfuric acid and methanol into A agent according to the weight ratio of 1:25;
[0057] 3. Add agent A to liquid 1 at a volume ratio of 1:6, control the temperature at 75°C, stir and react for 2 hours to form agent B;
[0058] 4. After agent B is allowed to stand for 13 hours, light brownish yellow solution F1 is released, and the rest becomes liquid 2.
[0059] 5. Prepare caustic soda and methanol at a weight ratio of 1:25 to form agent C;
[0060] 6. Heat liquid 2 to 75°C, add agent C to liquid 2 in a volume ratio of 1:8, stir and mix for reaction for 2 hours, keep it warm and stand for 3 hours, and release bottom layer solution F2.
[0061] 7. Extract and condense the methanol under negative pressure, continue to stir and keep the temperature for 60 minutes during this process, then cool down naturally.
[0062] 8. After standing for 13 hours, the bottom layer solution F3 (light brownish yellow) is rel...
Embodiment 3
[0067] 1. The recovered natural oil is filtered, dried and precipitated and heated to 85°C to become liquid 1;
[0068] 2. Formulate sulfuric acid and methanol to form A agent at a weight ratio of 1:35;
[0069] 3. Add agent A to liquid 1 at a volume ratio of 1:10, control the temperature at 85°C, stir and react for 0.5 hours to form agent B;
[0070] 4. After agent B is allowed to stand for 12 hours, the bottom color light brownish yellow solution F1 is released, and the rest becomes liquid 2.
[0071] 5. Prepare caustic soda and methanol at a weight ratio of 1:35 to form agent C;
[0072] 6. Heat liquid 2 to 85°C, add agent C to liquid 2 in a volume ratio of 1:10, stir and mix for 0.5 hours, keep it for 4 hours, and release the bottom layer solution F2.
[0073] 7. Extract and condense the methanol under negative pressure, continue to stir and keep the temperature for 30 minutes during this process, then cool down naturally.
[0074] 8. After standing for 12 hours, the bottom layer solu...
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