Active materials for photoelectric devices and devices that use the materials
An electro-optic device, device technology, applied in the field of conjugated polymer as active layer material for electro-optic devices
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Embodiment 1
[0073] Poly(3,3'-bis(2-ethylhexyl)-silylene-2,2'-bithiophene-5,5'-diyl)-alt-benzo[c][1,2, 5] Synthesis of thiadiazole (HSi-1)
[0074] The synthetic route to this polymer HSi-1 is shown in the scheme below.
[0075]
[0076] 4.78g (10mmol) of 3,3',5,5'-tetrabromo-2,2'-bithiophene (the compound in the scheme above) synthesized by the reported method [Heterocycles; 1991(32), 1805-1812] 1) Dissolve in 150ml ultra-dry THF, cool the solution to -90°C through a liquid nitrogen-methanol bath and stir for 15 minutes. Then 8 ml of a solution of butyllithium in hexane (2.5 mol / L) was added dropwise over 1 hour, and the reaction was stirred for a further 15 minutes. Then 2.7 g of trimethylchlorosilane (25 mmol) was added in one portion and the cooling bath was removed to allow the reaction to warm to ambient temperature. The reaction was then poured into water and extracted several times with ether. Volatile materials were removed in vacuo. The residue was purified by recrystalli...
Embodiment 2
[0082] Fabrication and Characterization of Polymer Solar Cells Using HSi as Active Layer Material
[0083] Polymer HSi (30 mg) was dissolved in chlorobenzene to make 20 mg ml -1 solution and then blended with 60% by weight PCBM.
[0084] Polymer solar cells are fabricated on transparent indium tin oxide (ITO)-coated glass substrates. A thin layer of conductive polymer: poly(3,4-ethylenedioxythiophene) (PEDOT:PSS) doped with poly(styrene sulfonate) was spin-coated on the ITO surface as a better interface. The thickness of the PEDOT:PSS layer was about 30 nm as measured with a Dektek profilometer. Thin layers were then spin-coated from the solution prepared above. Then at about 10 -4 Thin layers of calcium and aluminum are sequentially evaporated at a pressure of Pa. The test is filled with N 2 A xenon lamp solar simulator calibrated with a silicon diode (with KG5 visible light filter) calibrated in the National Renewable Energy Laboratory (NREL) was irradiated at AM 1.5G ...
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