Method for detecting multiple transgenic plants based on silica spheres coded by fluorescence quantum dots (QDs)
A technology of silica spheres and fluorescent quantum dots, applied in chemical instruments and methods, fluorescence/phosphorescence, luminescent materials, etc., to achieve the effect of simple operation, regular shape, and good monodispersity
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[0048] The 535nmQDs, 602nmQDs, 629nmQDs, and 650nmQDs quantum dots used were purchased from Wuhan Jiayuan Co., Ltd. The following different volume ratios were used:
[0049] 535nmQDs: 629nmQDs=2:1,
[0050] 535nmQDs: 629nmQDs=1:2,
[0051] 535nmQDs: 602nmQDs: 650nmQDs=1:1:2,
[0052] Preparation of 535nmQDs: 602nmQDs: 650nmQDs=1:2:2 coded silica spheres and their application in the detection of transgenic corn, soybean, rapeseed and cotton.
[0053] 1. Fabrication of fluorescent quantum dot-encoded silica spheres
[0054] (1) Mix 15 mL of Triton and 15 mL of n-hexanol for 10 minutes, add 60 mL of cyclohexane, and stir for 20 minutes.
[0055] (2) Mix 1400 μL 535nm QDs and 700 μL 629nm QDs evenly, add to the above solution, stir evenly for 30 min, and configure a microemulsion system.
[0056] (3) Add 2mL of ammonia water to the above system, mix for 30min, add 2mL of TEOS and 2mL of APTES, and hydrolyze for 12h.
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