Polymorphic detection specific primers and liquid phase chip in 8 q 24 section of chromosome
A technology of polymorphism detection and liquid phase chip, which is applied in the field of molecular biology, can solve the problems of poor repeatability and unusability, and achieve good signal-to-noise ratio, consistent detection effect, and low cross-reaction rate
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Embodiment 1
[0021] Example 1 The liquid-phase chip for detecting the polymorphism of chromosome 8q24 segment mainly includes:
[0022] 1. ASPE Primers
[0023]Specific primer sequences were designed for the wild-type and mutant types of 11 common genotypes G83T, C140A, C160T, G99A, C202A, C296T, A125C, T119C, C149A, C193T and G201T on chromosome 8q24 segment. ASPE primers consist of "Tag sequence + specific primer sequence". ASPE primer sequences are shown in the table below:
[0024] Table 1 ASPE primer sequence (Tag sequence + specific primer sequence) of chromosome 8q24 segment
[0025]
[0026]
[0027]
[0028] Each ASPE primer includes two parts, the 5' end is a specific tag sequence for the anti-tag sequence on the corresponding microsphere, and the 3' end is a mutant or wild-type specific primer fragment (as shown in the above table 1). All ASPE primers were synthesized by Shanghai Sangon Bioengineering Technology Service Co., Ltd. Each synthesized primer was prepared...
Embodiment 2
[0042] Example 2 Detection of Samples Using a Chromosome 8q24 Segment Detection Liquid Chip
[0043] The formula of described various solutions is as follows:
[0044] 50mM MES buffer (pH5.0) formula (250m1):
[0045]
[0046] 2×Tm hybridization buffer
[0047] Reagent
[0048] Store at 4°C after filtration.
[0049] ExoSAP-IT kit was purchased from US USB Company.
[0050] Biotin-labeled dCTP was purchased from Shanghai Sangon Bioengineering Technology Service Co., Ltd.
[0051] 1. Sample DNA extraction:
[0052] Refer to the relevant methods of DNA extraction in "Molecular Cloning" to obtain the DNA to be detected.
[0053] 2. PCR amplification of samples to be tested
[0054] 11 pairs of primers were designed, and multiplex PCR amplified 11 target sequences of 11 common genotypes G83T, C140A, C160T, G99A, C202A, C296T, A125C, T119C, C149A, C193T and G201T in one step, respectively containing the chromosome 8q24 segment , the product sizes are 273bp, 342b...
Embodiment 3
[0101] Example 3 Detection of Chromosome 8q24 Segment Polymorphism Site by Liquid Chip with Different ASPE Primers
[0102] 1. Design of liquid phase chip preparation (selection of Tag sequence and Anti-Tag sequence)
[0103] Taking the liquid-phase chip for detection of site mutations in the C160T and C202A segments of chromosome 8q24 as an example, the specific primer sequences at the 3' end of the ASPE primers were designed for the wild-type and mutant types of C160T and C202A, respectively, and the Tag sequence at the 5' end of the ASPE primers was selected. From SEQ ID NO.1-SEQ ID NO.22, correspondingly, the anti-tag sequence coated on the microsphere and complementary to the corresponding tag sequence is selected from SEQ ID NO.45-SEQ ID NO.66. The specific design is shown in the following table (Table 9). The synthesis of ASPE primers, microspheres coated with anti-tag sequences, amplification primers, detection methods, etc. are as described in Example 1 and Example 2...
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