curable resin composition
A technology of curable resin and composition, applied in nonlinear optics, coatings, instruments, etc., can solve problems such as insufficient planarization and poor display of liquid crystal display devices
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[0170] The present invention will be described in more detail below by way of examples. "%" and "parts" in the examples are % by mass and parts by mass unless otherwise specified.
Synthetic example 1
[0172] Into a flask equipped with a reflux condenser, a dropping funnel, and a stirrer, nitrogen was flowed in at 0.02 L / min to form a nitrogen atmosphere, 140 parts of diethylene glycol ethyl methyl ether was charged, and heated to 70° C. while stirring. Next, prepare 40 parts of methacrylic acid; and the mixture of monomer (I-1) and monomer (II-1) {monomer (I-1) in the mixture: the mole of monomer (II-1) Ratio = 50:50} 360 parts of a solution dissolved in 190 parts of diethylene glycol ethyl methyl ether was dropped into a flask kept at 70°C over 4 hours using a dropping funnel.
[0173]
[0174] On the other hand, a solution obtained by dissolving 30 parts of the polymerization initiator 2,2'-azobis(2,4-dimethylvaleronitrile) in 240 parts of diethylene glycol ethyl methyl ether was used with another drop The liquid pump dripped into the flask over 5 hours. After the dropwise addition of the polymerization initiator solution was completed, it was kept at 70° C. for 4 hou...
Synthetic example 2
[0176] In a flask equipped with a reflux condenser, a dropping funnel, and a stirrer, nitrogen was flowed in at 0.02 L / min to form a nitrogen atmosphere, and 200 parts by mass of 3-methoxy-1-butanol and 3-methoxyacetic acid were charged. 105 parts by mass of butyl butyl ester was heated to 70° C. while stirring. Next, prepare 60 parts of methacrylic acid; and a mixture of monomer (I-1) and monomer (II-1) {monomer (I-1) in the mixture: moles of monomer (II-1) Ratio = 50:50} 240 parts of a solution dissolved in 140 parts of 3-methoxybutyl acetate was dropped into a flask kept at 70°C over 4 hours using a drip pump.
[0177] On the other hand, a solution obtained by dissolving 30 parts of the polymerization initiator 2,2'-azobis(2,4-dimethylvaleronitrile) in 225 parts of 3-methoxybutyl acetate was used in another The dropping funnel was dropped into the flask over 4 hours. After the dropwise addition of the polymerization initiator solution was completed, it was kept at 70° C. ...
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