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Method for processing raw material of isostatic pressing clay-graphite crucible

A graphite crucible and raw material processing technology, which is applied in the field of raw material processing of hydrostatic clay graphite crucible, can solve the problems of poor strength of dry-processed molded body, difficult operation, complicated phenolic resin treatment, etc., achieves good molding effect, avoids process rejection rate, The effect of excellent sintering properties

Active Publication Date: 2014-12-24
CHINA SCI HENGDA GRAPHITE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The isostatic pressing molding technology adopts dry molding, that is, it adopts dry powder molding. The clay graphite crucible raw material is a coarse particle material, and the largest particle is millimeter-sized. The dry molding body has poor strength and is not easy to operate. In patent 88102686.7, it is proposed to use the method of adding phenolic resin to obtain molding strength, but the post-treatment of phenolic resin is complicated

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A method for processing raw materials of an isostatic clay graphite crucible, specifically comprising the following steps:

[0025] 1) In parts by weight, take 550kg of flake graphite, 500kg of silicon carbide with a particle size of 150 microns, and 250 kg of clay. The clay is pre-pulverized into -75 micron powder, mixed for 40 minutes with dry material, mixed with 250 kg of water, wet mixed for 40 minutes, and then Rolling, rolling for 8 hours, and then trapping the material at 20±5°C for 15 days, repeating the rolling and trapping process once, keeping the moisture content of the material at 20±5% during the rolling process, and then using a low-speed pulverizer to crush the material Carry out thinning treatment and break up materials;

[0026] 2) Spread and bake the evacuated material obtained in step 1) on a kang at 80°C until the weight percentage of water in the material is 5%, and break the material with a high-speed coulter mixer until there is no formation bet...

Embodiment 2

[0029] A method for processing raw materials of an isostatic clay graphite crucible, specifically comprising the following steps:

[0030] 1) In parts by weight, take 550kg of flake graphite, 500kg of wax stone with a particle size of -4mm, and 200kg of clay. The clay is pre-pulverized into -75 micron powder, mixed with dry material for 30 minutes, added with 250kg of water, mixed evenly, wet mixed for 45 minutes, and then Carry out rolling and compacting for 10 hours, then trap the material at 20±5°C for 15 days, repeat the rolling and trapping process once, keep the moisture content of the material at 20±5% during the rolling process, and then use a low-speed pulverizer to crush the The material is thinned and dispersed;

[0031] 2) Spread and bake the material obtained in step 1) on a kang at 90°C until the weight percentage of water in the material is 8%, and break up the material with a high-speed coulter mixer until there is no agglomeration between the particles , to o...

Embodiment 3

[0034] 1) In parts by weight, take 500kg of flake graphite, 300kg of calcined kaolinite with a particle size of -2 mm, 200 kg of silicon carbide with a particle size of 150 microns, and 230 kg of clay. The clay is pre-pulverized into -75 micron powder, mixed with dry material for 45 minutes, and added with 250 kg of water Mix evenly, wet mix for 35 minutes, then roll and compact for 10 hours, then trap the material at 20±5°C for 15 days, repeat the process of rolling and trapping once, and keep the moisture content of the material at 20± during the rolling process 5%, and then use a low-speed pulverizer to thin the material and break it up;

[0035] 2) Spread and bake the material obtained in step 1) on a kang at 80°C until the weight percentage of water in the material is 7%, and break up the material with a high-speed coulter mixer until there is no agglomeration between the particles , to obtain the raw material for forming the isostatic clay graphite crucible.

[0036] Pu...

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Abstract

The invention discloses a method for processing a raw material of an isostatic pressing clay-graphite crucible. The method comprises the steps of: 1, adding water in the following raw materials in parts by weight: 35-55 parts of crystalline flake graphite, 20-50 parts of aggregate and 15-25 parts of clay, uniformly mixing, grinding, ageing for 10-15 days, then repeatedly rolling and ageing, and then carrying out draining; and 2, drying a material obtained in the step 1 at a temperature of 100 DEG C until the weight percent of water in the material is 5 percent and 8 percent, and finally dispersing to obtain the raw material of forming the isostatic pressing clay-graphite crucible. The raw material made by adopting the method disclosed by the invention has enough wet strength, a certain plasticity, good forming effect, and excellent sintering property, and ensures the strength and hardness of the crucible.

Description

technical field [0001] The invention relates to the field of clay-graphite crucible processing, in particular to a raw material processing method for an isostatic clay-graphite crucible. Background technique [0002] Clay graphite crucible is a tooling equipment for non-ferrous metal smelting, which needs to have good refractory properties, and also has good uniform heat conduction and no pollution to smelted metals. Clay graphite crucibles have these characteristics, which have a lot to do with the selection of raw materials, and the process is also the key. [0003] The most critical part of the clay-graphite crucible manufacturing process is the clay treatment process. The clay-graphite crucible is molded and sintered to obtain the required properties, all of which are obtained through the combination of clay. Using different process methods, the dispersion of crucible flake graphite, aggregate, and clay are different, the accumulation of powder or particles inside the c...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66
Inventor 傅云峰杨帆周琰
Owner CHINA SCI HENGDA GRAPHITE