Method for recovering saponin from saponin mother solution
A saponin and mother liquor technology, applied in steroids, organic chemistry and other directions, can solve the problems of polluting the environment, high viscosity of mother liquor, affecting the yield and quality of saponin products, etc., to save natural resources and reduce pollution.
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Embodiment 1
[0012] Weigh 100 kg of saponin mother liquor jelly (the saponin content is 33.9% as detected by high performance liquid phase method). Add 300 kg of compound degreasing solution, heat to 95°C, stir for one hour, suction filter while hot, rinse with 200 liters of deionized water until the water is neutral. The solids were dried and pulverized to obtain 35.8 kg of the product, with a melting point of 197-201°C and a saponin content of 95.3% as detected by HPLC. The recovery rate of saponin was 100.6%.
Embodiment 2
[0014] Weigh 100 kilograms of saponin mother liquor jelly (the saponin content is 27% as detected by high performance liquid phase method). Add 200 kg of compound degreasing solution, heat to 95°C, stir for one hour, suction filter while hot, rinse with 180 liters of deionized water until the water is neutral. The solids were dried and pulverized to obtain 31.4 kg of the product, with a melting point of 193-199°C and a saponin content of 86.2% as detected by HPLC. 27 kg of the product was obtained by recrystallization with acetone, the detected melting point was 200-205 degrees Celsius, and the saponin content was 98.2% as detected by HPLC. The recovery rate of saponin was 98.3%.
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