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A kind of road asphalt prepared from coal tar and preparation method thereof

A technology for road asphalt and coal tar pitch, applied in the field of road asphalt and its production technology, can solve the problems of high raw material transportation cost and production cost, high production cost and raw material transportation cost, and difficulty in matching the output of coal tar pitch, so as to achieve anti-aging of products. High performance, improved anti-aging properties, easy to scale production

Active Publication Date: 2016-04-20
山西中科化美科技有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The above two types of road asphalt use coal tar pitch and petroleum pitch as the main raw materials. Since the main production areas of coal tar pitch and petroleum pitch are not concentrated, the raw material transportation costs and production costs of the two road asphalts are relatively high, and it is difficult to break through the supply of raw materials. Limits to large-scale industrial production
[0007] Some of the above-mentioned road asphalt prepared from coal tar pitch need to add petroleum asphalt as the main raw material, the production cost and raw material transportation cost are high, the source of raw material has the risk of market uncertainty, and it is difficult to produce on a large scale; all of them only use coking solvent oil as the solvent, Evaporation loss is large, and the performance of road construction oil decreases obviously after aging; additives such as synthetic resin and synthetic rubber need to be added, and the production cost is high; the process is relatively complicated, and the output is difficult to increase, which is difficult to match with the increasing output of coal tar pitch

Method used

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  • A kind of road asphalt prepared from coal tar and preparation method thereof
  • A kind of road asphalt prepared from coal tar and preparation method thereof
  • A kind of road asphalt prepared from coal tar and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Add 70 parts of coal tar pitch 1 into the reactor, and raise the temperature in the reactor to 100°C to soften the coal tar pitch; then add 3 parts of waste rubber powder, 30 parts of coking solvent naphtha, 1.25 parts of 2,2,4-trimethyl -1,2-dihydroquinoline polymer, and the temperature in the reactor was raised to 200°C and mixed for 1.5h.

[0028] The quality index of the prepared road polymer modified coal tar pitch is as follows:

[0029]

[0030] The coking solvent oil used in this example is anthracene oil 1, and the distillate before 400°C accounts for 92.2%.

Embodiment 2

[0032] Add 60 parts of coal tar pitch 1 into the reactor, and raise the temperature in the reactor to 100°C to soften the coal tar pitch; then add 3 parts of waste rubber powder, 2.5 parts of N-phenyl-N'-isopropyl-terephthal Amine, 30 parts of coking mineral spirits and 10 parts of high boiling point low vapor pressure oil and the temperature inside the reactor was raised to 220°C and mixed for 1.5h.

[0033] The quality index of the prepared road polymer modified coal tar pitch is as follows:

[0034]

[0035] The coking solvent oil used in this example is anthracene oil 1, and the distillate before 400°C accounts for 92.2%.

[0036] The high boiling point and low vapor pressure oil used in this example has an initial boiling point of 303° C. and a saturated vapor pressure of 3.5 Pa at 100° C.; the high boiling point and low vapor pressure oil is waste tire oil.

Embodiment 3

[0038] Add 60 parts of coal tar pitch 1 into the reactor, and raise the temperature in the reactor to 100°C to soften the coal tar pitch; then add 3 parts of waste rubber powder, 1.25 parts of 2,2,4-trimethyl-1,2-di Hydrogenated quinoline polymer, 1.25 parts of N-phenyl-N'-isopropyl-p-phenylenediamine, 20 parts of coking solvent oil and 20 parts of high boiling point and low vapor pressure oil and the temperature in the reactor is raised to 220°C After mixing for 2 hours; finally, the temperature in the reactor was lowered to 100°C and kept constant, and 1.25 parts of high boiling point and low vapor pressure oil was added and mixed for 0.5 hours.

[0039] The quality index of the prepared road polymer modified coal tar pitch is as follows:

[0040]

[0041] The coking solvent oil used in this example is anthracene oil 2, and the distillate before 400°C accounts for 96.4%.

[0042] The high boiling point and low vapor pressure oil used in this example has an initial boilin...

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Abstract

The invention relates to a road asphalt prepared from waste rubber-modified coal asphalt and a production process of the road asphalt. The invention overcomes the defects of the prior art, provides the road asphalt prepared from the coal asphalt and the production process of the road asphalt, and is characterized by using the coal asphalt as a raw material, adding waste rubber powder and an anti-aging agent as modifiers, adding a coking solvent oil and an oil with high boiling point and low steam pressure as solvents, and recycling the oil with high boiling point and low steam pressure finally. The adopted technical scheme is that the road asphalt prepared from the coal asphalt comprises the following raw materials in parts by weight: 50-80 parts of the coal asphalt, 10-40 parts of the coking solvent oil, 2-6 parts of the waste rubber powder, 10-30 parts of the oil with high boiling point and low steam pressure, and 0.03-3 parts of the anti-aging agent. According to the preparation method, the prescription and the production process are improved, the raw material cost is low, the resource is wide, and the method is suitable for large-scale production; and the prepared road asphalt product has the characteristics that the anti-aging performance is high, the quality loss after the aging is low, the needle penetration ratio is high, and the residual ductility is high.

Description

technical field [0001] The invention relates to a road asphalt and a production process thereof, in particular to a road asphalt prepared from waste rubber modified coal tar pitch and a production process thereof. Background technique [0002] my country's coke output has been ranked first in the world. According to incomplete statistics, the national coke output in 2011 was 427 million tons, a year-on-year increase of 11.7%. From January to October 2012, the national coke output was 369 million tons, a year-on-year increase of 4.2%. In 2011, the national output of high-temperature coal tar was about 17.5 million tons. In addition, medium and low temperature dry distillation of low-rank coal has become a hot spot in my country's coal chemical industry in recent years, and the production of medium and low temperature coal tar has also increased year by year. [0003] Coal tar pitch is a product obtained after distillation of coal tar, and its yield is about 55% to 60% of th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L95/00C08L21/00C08K11/00C08K5/3437C08K5/18
Inventor 王磊张伟冯硕
Owner 山西中科化美科技有限责任公司