Silver-based electrical contact material
一种电接触材料、银基的技术,应用在触点、电路、电开关等方向,能够解决难以实现均匀的分散、不可行、增加材料制造成本等问题
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[0015] The preparation method of silver-based electrical contact material of the present invention comprises the following steps:
[0016] (a) providing a carbonaceous mesophase solution;
[0017] (b) adding a silver source to the carbonaceous mesophase solution and stirring to obtain a mixture;
[0018] (c) removing the solvent from the mixture to obtain a solid;
[0019] (d) heat-treating the solid to obtain a silver-based electrical contact material.
[0020] The preparation method and characteristics of the silver-based electrical contact material of the present invention will be described in detail below in conjunction with specific processes.
[0021] (1) Carbonaceous mesophase solution
[0022] The carbonaceous mesophase solution provided in the method of the present invention provides the carbonaceous substance in the electrical contact material as a raw material. This carbonaceous mesophase solution is prepared by dissolving the carbonaceous mesophase in a suita...
Embodiment 1
[0075] Provides a carbonaceous mesophase solution
[0076] The carbonaceous mesophase can be obtained according to known methods. The biomass-derived carbonaceous mesophase powder used in the present invention was obtained from Shandong Qufu Tianbojing Carbon Technology Co., Ltd.
[0077] The carbonaceous mesophase solution was prepared as follows:
[0078] The biomass-derived carbonaceous mesophase powder is placed in ethanol, stirred and dissolved, and left standing to obtain a carbonaceous mesophase solution. The concentration of the solution was determined by drying, and an appropriate amount of solvent was added for dilution according to the measurement results to obtain a carbonaceous mesophase solution with a concentration of 4%. Measure an appropriate amount of solvent and add, obtain a series of ethanol solutions of carbonaceous mesophase after fully stirring, the concentration of carbonaceous mesophase is respectively 0.4%, 0.04%, and 1%, 0.1% and 0.01% (all by w...
Embodiment 2
[0082] Embodiment 2 prepares solid-liquid mixture
[0083] Immerse the chemical silver powder and the atomized silver powder in the carbonaceous mesophase ethanol solution of different concentrations prepared in Example 1 respectively, after fully mixing, evaporate and remove the ethanol, thus obtaining the silver-carbon composite body, wherein the carbonaceous The concentrations of the mesophase solutions are shown in Table 1.
[0084] EDX qualitatively analyzed the coating amount of carbonaceous silver powder (expressed in weight %) obtained by impregnating atomized silver powder and chemical silver powder with different concentrations of carbonaceous mesophase solutions, and the results are shown in Table 1 below.
[0085] Table 1: Qualitative analysis of carbonaceous mesophase solution by EDX to compare the impregnation coating amount of atomized silver powder and chemical silver powder
[0086]
[0087] From the EDX analysis results in Table 1, it can be clearly seen ...
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