Polyethylene glycol bisalkenyl succinate monoalkyl ester and preparation method thereof
A technology of monoalkyl alkenyl succinate and polyethylene glycol, which is applied in the field of steel plate rolling oil, can solve the problems of complex rolling oil formulation, and achieves the advantages of solving the problem of formula complexity and excellent emulsifying performance. Effect
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[0028] In a three-necked flask with a reflux condenser, add 265 grams of dodecenyl maleic anhydride in a nitrogen atmosphere, add 1% toluenesulfonic acid of the weight of dodecenyl maleic anhydride as a catalyst, then add 186 gram of lauryl fatty alcohol, and 10% dehydrating agent in total, heated up to 115-120°C under stirring, and analyzed the acid value of the reaction system every 0.5 hours during the reaction until the acid value remained unchanged, and the reaction time was 4-5 hour; then add 102 grams of polyethylene glycol (average molecular weight 200), and heat up to 150-160°C under stirring. During the reaction, analyze the acid value of the reaction system every 0.5 hours until the acid value remains unchanged. The reaction time is 6-8 hours, until no water is distilled off, and then the solution is decompressed to make the vacuum of the system reach 0.07-0.08MPa, and the solvent xylene is distilled off. The product of the reaction is the product.
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