Glass softening point testing device

A glass softening point and testing device technology, applied in the investigation phase/state change and other directions, can solve the problem of lack of optical fiber drawing process and the inability to obtain the sample length accurately, and achieve the effect of simple and cheap device operation and accurate data.

Active Publication Date: 2015-03-04
HUBEI NEW HUAGUANG NEW INFORMATION MATERIALS CO LTD
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Problems solved by technology

But generally speaking, the diameter of the test sample required by the above two test devices and test methods is not greater than 5mm, and the heating rate is relatively fast at 5±1°C/min, so when the test sample is heated by radiation, it cannot be accurately The value of the change of the le

Method used

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[0018] The present invention will be further described below with reference to the drawings and embodiments.

[0019] The softening point test device described in the technical solution of the present invention is as follows Figure 4 As shown, it is mainly composed of heating furnace 6, upper protective cover 4, lower protective cover 5, sample holder 9, test pressure rod 11, and load 1. The sample holder 9 is located at the bottom of the lower protective cover 5, and the test sample 10 is placed On the sample holder 9. The sample 10 to be tested is located in the middle of the heating furnace 6, and the thermocouple 7 for temperature measurement is placed in the sample holder 9 at the lower part of the sample 10 to be tested. And the upper protective cover 4, the lower protective cover 5, the sample holder 9 and the test pressure rod 11 are made of quartz material or zero-expansion glass material, so that the lower thermal expansion coefficient of quartz material and zero-expan...

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Abstract

The invention provides a glass softening point testing device, and belongs to the technical field of testing of optical materials. The problem that data are not accurate when a small sample is tested in an existing softening point testing method is solved. The softening point testing is mainly characterized in that an upper protection cover, a lower protection cover, a sample bracket and a testing pressing rod are made of quartz or zero-expansion glass, wherein the lower protection cover is fixed in a heating furnace; a V-shaped groove is formed in the upper part of the sample bracket and a thermoelectric couple hole is formed in the side face of the sample bracket; the sample bracket is arranged at the center of the bottom in the lower protection cover and a thermoelectric couple is arranged in the thermoelectric couple hole; the testing pressing rod penetrates into the sample bracket from a fixed hole in the upper end of the upper protection cover; a load is arranged at the upper end of the testing pressing rod; the testing pressing rod is located outside the upper protection cover and a transverse pointer is fixedly arranged on the rod; and the glass softening point testing device further comprises a graduated disc matched with the pointer. The glass softening point testing device has the characteristics that the operation is simple and testing data are relatively accurate when being compared with data needed by actual production; and the glass softening point testing device is mainly used for testing a softening point of a relatively large glass sample.

Description

technical field [0001] The invention belongs to the technical field of optical material testing, and in particular relates to a glass softening point testing device. It can accurately test the softening temperature of glass, so as to provide reliable data basis for the drawing process of glass optical fiber. Background technique [0002] With the fierce competition and development of the optoelectronic product market, glass optical fibers are more and more widely used in medical, aviation, military, lighting and decoration industries. The glass softening point has become a very important evaluation parameter for optical fiber glass. Currently, commonly used softening point testing devices include quartz dilatometers as shown in Figure 1 and wire drawing devices such as image 3 shown. The test principle of the quartz dilatometer is to use the differential method, that is, to use the material with good thermal stability—quartz glass (rod and tube) at higher temperatures, wh...

Claims

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Application Information

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IPC IPC(8): G01N25/04
Inventor 胡向平段晓涛戎俊华霍金龙赵仲勋
Owner HUBEI NEW HUAGUANG NEW INFORMATION MATERIALS CO LTD
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