Method for reducing energy consumption of oxidizing reaction unit of phenol-acetone device
An oxidation reaction, phenol acetone technology, applied in chemical instruments and methods, preparation of oxygen-containing compounds, preparation of peroxy compounds, etc., can solve the problem of high energy consumption, and achieve the effect of increasing pipeline resistance and increasing power consumption
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[0018] [Example 1]
[0019] In such figure 1 In the device process shown, the cumene raw material feed line (1) with a mass content of cumene of 66.1% exchanges heat with the reflux material of the oxidation tower through the oxidation tower heat exchanger (2), and the heated cumene The benzene raw material is preheated to 55°C by the preheater (4) and then enters the oxidation tower (6), and undergoes oxidation reaction with the air introduced through the air inlet line (7); the top of the oxidation tower (6) contains a small amount of cumene The tail gas with water is sent to the outside through the gas phase outlet pipeline (5); the liquid phase material containing cumene and cumene hydrogen peroxide in the oxidation tower (6) is pressurized by the booster pump (8), and part of the liquid phase The material is sent as an oxidation product, and a part of the oxidation product (9) enters the oxidation tower heat exchanger (2) through the return line to exchange heat with the cu...
Example Embodiment
[0024] [Example 2]
[0025] According to the conditions and steps described in Example 1, the production scale of phenol acetone was changed to 200,000 tons / year. It can reduce the consumption of low-pressure steam by 3.80 tons / hour and the consumption of circulating cooling water by 203 tons / hour.
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[0026] [Example 3]
[0027] According to the conditions and steps described in Example 1, only the production scale of phenol acetone was changed to 350,000 tons / year. It can reduce the consumption of low-pressure steam by 6.65 tons / hour and reduce the consumption of circulating cooling water by 354 tons / hour.
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