Preparation method of nano-porous carbon aerogel of super capacitor
A supercapacitor and nanoporous carbon technology, which is applied in the manufacture of hybrid/electric double layer capacitors, hybrid capacitor electrodes, hybrid capacitor electrolytes, etc., can solve the problems of activated carbon specific capacity and specific surface area limitations, difficult specific capacity, etc., to achieve good specific capacity , the effect of high application value
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[0014] A kind of preparation method of the nanoporous carbon airgel of supercapacitor, any following metal ion Al 3+ , Li + ,Zn 2+ ,Cu 2+ ,Pb 2+ Underpotential deposition on the surface of carbon aerogels provides Faraday quasi-capacitance for electrochemical double-layer capacitors. Specifically include the following steps:
[0015] Step 1. Add a concentration of 3.0 to 4.0×10 to the KOH electrolyte of the supercapacitor -2 mol / L of any of the following ionic solutions Al 3+ , Li + ,Zn 2+ ,Cu 2+ , Pb 2+ ;
[0016] Step 2, using the above-mentioned ion solution to modify the carbon airgel powder, so that the above-mentioned ions are deposited in the micropores of the carbon aerogel, thereby obtaining the nanoporous carbon aerogel of the supercapacitor.
[0017] In this step, there are two ways to modify the carbon airgel powder:
[0018] Method 1 is: will use Pb (NO 3 ) 2 The solution soaks carbon aerogels under vacuum conditions, making the Pb(NO 3 ) 2 The sol...
Embodiment 1
[0021] Add 3.1×10 -2 mol / LPb 2+ Pb(Ac) 2 , through the supercapacitor charging and discharging activation process, the metal ions are converted into Pb(OH) 2 deposited on the carbon aerogel surface.
Embodiment 2
[0023] Add 4.0×10 -2 mol / LPb 2+ Pb(Ac) 2 , through the supercapacitor charging and discharging activation process, the metal ions are converted into Pb(OH) 2 deposited on the carbon aerogel surface.
[0024] It is very meaningful to use the Faraday quasi-capacitance to increase the capacitance of double-layer capacitors. The invention selects metal ions capable of underpotential deposition on the surface of the carbon airgel material to increase the specific capacitance of the carbon airgel electrode, thereby increasing the capacity of the supercapacitor. Single double-layer capacitors are based on high specific surface area materials, such as the double-layer capacitance at the solid / liquid surface of carbon aerogel. Similar to traditional capacitors, the storage of electric energy is based on the electrolytic double-layer capacitor at the horizontal electrode / solution interface. Based on charging within the layer, when a DC voltage is applied to the interface of the elec...
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