Preparation method of high-aging-resistance rubber asphalt
A rubber asphalt, high-resistance technology, applied to building components, building insulation materials, buildings, etc., can solve the problems of waste tires that are difficult to degrade, mosquitoes spread diseases, occupy large land, etc., to improve low-temperature crack resistance and not easy to freeze , good weather resistance
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Embodiment 1
[0017] The preparation method of high anti-aging rubber asphalt comprises the following steps:
[0018] ①Wash the waste rubber, dry it naturally, and remove metal and fiber debris after preliminary crushing;
[0019] ②Crush the waste rubber after the above pretreatment into rubber powder, add ferrous sulfate, and activate it at 130°C for 3 hours; the amount of ferrous sulfate added is 0.1% of the mass of rubber powder;
[0020] ③Add the asphalt matrix preheated to 180°C to the product of step ②, then add the rubber regeneration reducing agent PTC-R and the antioxidant pentaerythritol dioctadecyl phosphite, mix in an open mill, and react at 200°C for 3 hours. Obtain high anti-aging rubber asphalt; the addition amount of asphalt matrix is 3 times of rubber powder quality, the addition amount of rubber regeneration reducing agent PTC-R is 0.5% of rubber powder quality, the antioxidant pentaerythritol dioctadecyl phosphite The amount added is 0.5% of the rubber powder mass.
Embodiment 2
[0022] The preparation method of high anti-aging rubber asphalt comprises the following steps:
[0023] ①Wash the waste rubber, dry it naturally, and remove metal and fiber debris after preliminary crushing;
[0024] ②Crush the waste rubber after the above pretreatment into rubber powder, add ferrous nitrate, and activate it at 130°C for 3 hours; the amount of ferrous sulfate added is 0.5% of the mass of rubber powder;
[0025] ③Add the asphalt matrix preheated to 180°C to the product of step ②, and then add the rubber regeneration reducing agent PTC-R and the antioxidant 1,3,5-trimethyl-2,4,6-tri(3,5 -Di-tert-butyl-4-hydroxybenzyl)benzene, mixed in an open mill, and reacted at 200°C for 5 hours to obtain high anti-aging rubber asphalt; the amount of asphalt matrix added was 5 times the mass of rubber powder, and the rubber was regenerated and reduced The addition amount of the agent PTC-R is 1% of the rubber powder mass, and the antioxidant 1,3,5-trimethyl-2,4,6-tris(3,5-di-...
Embodiment 3
[0027] The preparation method of high anti-aging rubber asphalt comprises the following steps:
[0028] ①Wash the waste rubber, dry it naturally, and remove metal and fiber debris after preliminary crushing;
[0029] ②Crush the waste rubber after the above pretreatment into rubber powder, add ferrous nitrate, and activate at 130°C for 3 hours; the amount of ferrous sulfate added is 0.3% of the mass of rubber powder;
[0030] ③Add the asphalt matrix preheated to 180°C to the product of step ②, and then add the rubber regeneration reducing agent PTC-R and the antioxidant 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionic acid n- Stearyl alcohol esters were mixed in an open mill and reacted at 200°C for 4 hours to obtain high anti-aging rubber asphalt; the amount of asphalt matrix added was 4 times the mass of rubber powder, and the amount of rubber regeneration reducing agent PTC-R added was 0.8% of the rubber powder mass, and the addition of antioxidant 3-(3,5-di-tert-butyl-4-hydr...
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