Polystyrene heat conduction material and preparation method thereof
A polystyrene and thermally conductive material technology, applied in the field of polystyrene thermally conductive materials and their preparation, can solve the problems of high cost and easy occurrence of circuit failures, and achieve the effect of improving thermal conductivity efficiency
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Embodiment 1
[0033] A polystyrene heat-conducting material is made of components comprising the following parts by weight:
[0034]
[0035] Among them, polystyrene is high-impact polystyrene; the thermally conductive fiber is carbon fiber with a diameter of 6um; the thermally conductive whisker is graphite whisker; the thermally conductive filler is expandable graphite powder with hydroxyl groups on the surface; the coupling agent is γ-aminopropyl base triethoxysilane; lubricant calcium stearate; antioxidant three [2.4-di-tert-butylphenyl] phosphite.
[0036] The preparation method of the expandable graphite powder with hydroxyl groups on the surface is specifically, preparing a mixed acid solution of perchloric acid and nitric acid with a weight ratio of 1:20, adding commercially available graphite powder to the above mixed acid solution and dispersing by microwave at 55 Oxidative expansion treatment is carried out at a temperature of ℃, and after the treatment is completed, it is fil...
Embodiment 2
[0041] A polystyrene heat-conducting material is made of components comprising the following parts by weight:
[0042]
[0043] Among them, polystyrene is high-impact polystyrene; thermally conductive fiber is copper fiber with a diameter of 15um; thermally conductive whisker is silicon carbide whisker; thermally conductive filler is alumina; coupling agent is 3-aminopropyltrimethoxysilane ; The lubricant is epoxy soybean oil; the antioxidant is N, N'-bis-(3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionyl) hexamethylenediamine.
[0044] The preparation method of the above-mentioned polystyrene heat conducting material comprises the following steps:
[0045] (1) Weigh polystyrene, thermally conductive whiskers, thermally conductive fillers, coupling agents, and antioxidants by weight and add them to the weighing scale of the extruder, and add them to the extruder through the weighing scale, melt extrusion, and the extrusion temperature 160~200℃;
[0046] (2) The melt extrude...
Embodiment 3
[0048] A polystyrene heat-conducting material is made of components comprising the following parts by weight:
[0049]
[0050] Among them, polystyrene is high-impact polystyrene; the thermally conductive fiber is carbon fiber with a diameter of 20um; the thermally conductive whisker is four-needle zinc oxide whisker; the thermally conductive filler is expandable graphite powder with hydroxyl groups on the surface; the coupling agent is γ-aminopropylmethyldiethoxysilane; lubricant is naphthenic rubber oil; antioxidant is 2,6-di-tert-butyl-4-methylphenol.
[0051] The preparation method of the expandable graphite powder with hydroxyl groups on the surface is specifically, preparing a mixed acid solution of perchloric acid and nitric acid with a weight ratio of 1:20, adding commercially available graphite powder to the above mixed acid solution and dispersing by microwave at 55 Oxidative expansion treatment is carried out at a temperature of ℃, and after the treatment is comp...
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