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Ceramic core preparation method

A ceramic core and ceramic powder technology, which is applied in the field of precision casting ceramic core preparation, can solve problems such as core deformation, environmental protection, and no way to know, and achieve low plasticizer consumption, strong practicability, and stable performance Effect

Active Publication Date: 2015-10-21
DONGFANG TURBINE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The firing process is the most critical step affecting the quality of the ceramic core. Defects such as cracks, expansion, deformation, bubbles, peeling, etc., as well as physical properties such as flexural strength and firing shrinkage are closely related to the firing process, and the key to the firing process is It lies in the reasonable and precise control of roasting temperature and roasting time. This technical measure is a commercial secret in the industry and has no way of knowing.
On the other hand, the mechanical and thermodynamic properties of ceramic cores after firing often cannot meet the requirements of use. The common practice is to use silica sol or resin materials to perform high-temperature strengthening and low-temperature strengthening treatments. This method increases the complexity of the process. At the same time, it is not only not environmentally friendly, but also may cause adverse effects on the deformation of the core itself

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A method for preparing a ceramic core with high flexural strength, excellent creep resistance, and low shrinkage rate includes the following steps:

[0019] 1). Dry the ceramic powder raw materials at 105℃ for 4 hours. After drying, weigh 20kg of ceramic powder (the ratio of ceramic powder is the existing ratio) and place it in the V-type mixer Mix for 2h, then put it in an oven at 105℃ for 1h after mixing, then transfer it to a vacuum mixing mixer and keep it at a constant temperature at 90℃;

[0020] 2). Weigh oleic acid with 0.5% of the ceramic powder mass, about 0.1kg, and dissolve the oleic acid with 15 times the volume of absolute ethanol; spray the oleic acid ethanol solution evenly into the mixer (ie, vacuum mixing mixer) In the ceramic powder, stir, open the air outlet valve of the mixer, so that the absolute ethanol will gradually volatilize during the mixing process; fully stir for 17 hours, so that the outer surface of the ceramic powder is covered with a layer o...

Embodiment 2

[0026] A method for preparing a ceramic core with high flexural strength, excellent creep resistance, and low shrinkage rate includes the following steps:

[0027] 1). Dry the ceramic powder raw materials at 140℃ for 3h. After drying, weigh 20kg of ceramic powder (the ratio of ceramic powder is the existing ratio) and place it in the V-type mixer Mix for 2h, then put it in an oven at 140℃ for 1h after mixing, after a little cooling, transfer to a vacuum mixing mixer and keep it at a constant temperature at 80℃;

[0028] 2). Weigh oleic acid with 0.9% of the mass of the ceramic powder, about 0.18kg, and dissolve the oleic acid with 20 times the volume of absolute ethanol; spray the oleic acid ethanol solution evenly into the mixer (ie vacuum mixing mixer) In the ceramic powder, stir, open the air outlet valve of the mixer, so that the absolute ethanol will gradually volatilize during the mixing process; stir fully for 20 hours, so that the outer surface of the ceramic powder is cove...

Embodiment 3

[0033] A method for preparing a ceramic core with high flexural strength, excellent creep resistance, and low shrinkage rate includes the following steps:

[0034] 1). Dry the ceramic powder raw materials at 110℃ for 3.5 hours. After drying, weigh 20kg of ceramic powder (the ratio of ceramic powder is the existing ratio) and place it in the V-type mixer After mixing for 2 hours, put it in an oven at 110°C for 1 hour, then transfer it to a vacuum mixer and keep it at a constant temperature at 75°C;

[0035] 2). Weigh oleic acid with 0.4% of the ceramic powder mass, about 0.08kg, and dissolve the oleic acid with 10 times the volume of absolute ethanol; spray the oleic acid ethanol solution evenly into the mixer (ie, vacuum mixing mixer) In the ceramic powder, stir, open the air outlet valve of the mixer, so that the absolute ethanol will gradually volatilize during the mixing process; fully stir for 24 hours, so that the outer surface of the ceramic powder is covered with a layer of ...

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Abstract

The invention discloses a ceramic core preparation method. The method includes the steps that 1, ceramic powder is dried at the temperature ranging from 105 DEG C to 140 DEG C, and the dried ceramic powder is added to a vacuum mixing and stirring machine to be stirred at the constant temperature ranging from 75 DEG C to 95 DEG C; 2, oleic acid with the mass accounting for 0.3-1% of ceramic powder is weighed and dissolved with absolute ethyl alcohol with the volume being 10-30 times that of the oleic acid, a oleic acid ethanol solution is sprayed into the ceramic powder, stirring is conducted, a gas outlet valve is opened, and full mixing and gas discharging are conducted; 3, plasticizer with the mass accounting for 14-17% of the ceramic powder is weighed and added to the ceramic powder after being molten, and full stirring is conducted; 4, the stirring speed is lowered, the gas outlet valve is closed, vacuumizing is conducted till the pressure reaches over 88 KPa, a vacuum pump is closed, the stirring speed is recovered, and stirring is conducted continuously till the surface of the ceramic slurry is smooth, level and free of visible bubbles and particles; 5, the ceramic slurry is transferred to a core pressing machine to be stirred over 8 hours, pressing of a green ceramic core is conducted, and shaping and calcination are conducted on the pressed green ceramic core.

Description

technical field [0001] The invention relates to a method for preparing a precision casting ceramic core. Background technique [0002] In the precision casting process, especially in the near-net-shape investment casting process, the ceramic core is an important transition part to form a hollow casting, which directly determines the structural shape and molding accuracy of the casting cavity. Precision casting has high quality requirements for ceramic cores, and more than 50% of unqualified castings in precision casting are caused by unqualified ceramic cores. The unqualified reasons for ceramic cores are mainly reflected in insufficient flexural strength, poor creep resistance and large shrinkage. [0003] In addition to the physical properties of the material itself, such as chemical composition, particle size distribution, etc., the factors that affect the flexural strength, creep resistance and shrinkage of the ceramic core are the most critical factors that are the pre...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/622C04B35/632C04B35/634
Inventor 何建曾洪伍林杨功显杨照宏
Owner DONGFANG TURBINE CO LTD