Multilayered structure
A multi-layer structure, layer structure technology, applied in layered products, synthetic resin layered products, applications, etc., can solve problems such as leakage of fuel and tap water adhesion, and achieve excellent interlayer adhesion strength, excellent flexibility, Excellent oxygen barrier properties
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment
[0171] The present invention will be described more specifically by the following examples, but the present invention is not limited to these examples. In addition, various evaluations in Examples and Comparative Examples were performed by the following methods.
[0172] (1) Oxygen barrier properties (oxygen transmission rate)
[0173] According to JISK7126, using OX-TRAN (registered trademark) 2 / 21 (manufactured by MOCON Co., Ltd.), under the conditions of 23°C and 60%RH, the oxygen transmission rate (unit: cc / m 2 ·atm·day) for measurement.
[0174] (2) Pinhole resistance (number of pinholes)
[0175] Cut the produced stretched film with a total thickness of 25 μm into a square of 210 mm, use a Gelbo flex tester (manufactured by Rigaku Kogyo Co., Ltd.), set the axial direction of the Gelbo flex tester as the measurement direction, and set the temperature at 23° C. and 60% RH The number of pinholes when bending 1,000 times was measured under the environment. The pinhole m...
manufacture example 1
[0196] (Manufacture example 1) Manufacture of polyether polyamide b1
[0197] Put 650.37 g of adipic acid, 0.6125 g of sodium hypophosphite monohydrate, and 0.4266 g of sodium acetate into a reaction container with a volume of about 3 L equipped with a stirrer, a nitrogen gas inlet, and a condensed water outlet, and fully replace the container with nitrogen. Thereafter, the added components were melted at 170° C. while nitrogen gas was supplied into the container at 20 ml / min. While slowly raising the temperature in the container to 260° C., 588.04 g of m-xylylenediamine (MXDA) (manufactured by Mitsubishi Gas Chemical Co., Ltd.) and polyetherdiamine (manufactured by HUNTSMAN, USA, Jeffamine (registered trademark) were added dropwise into the container. ) ED-900, based on the product catalog of the HUNTSMAN company in the United States, the -OR in the aforementioned general formula (1-2) 1 -for-OCH(CH 3 )CH 2 -or-OCH 2 CH(CH 3 )-, the approximate number of x2+z2 is 6.0, th...
manufacture example 2
[0198] (Manufacture example 2) Manufacture of polyether polyamide b2
[0199] Put 584.60 g of adipic acid, 0.5933 g of sodium hypophosphite monohydrate, and 0.4133 g of sodium acetate into a reaction container with a volume of about 3 L equipped with a stirrer, a nitrogen gas inlet, and a condensed water outlet, and fully replace the container with nitrogen. Thereafter, the added components were melted at 170° C. while nitrogen gas was supplied into the container at 20 ml / min. While slowly raising the temperature in the container to 260° C., 516.52 g of m-xylylenediamine (MXDA) (manufactured by Mitsubishi Gas Chemical Co., Ltd.) and polyether diamine (manufactured by HUNTSMAN, USA, Jeffamine (registered trademark)) were added dropwise into the container. )XTJ-542, based on the product catalog of HUNTSMAN Company in the United States, the -OR in the aforementioned general formula (1-1) 1 -for-OCH(CH 3 )CH 2 -or-OCH 2 CH(CH 3 )-, the approximate number of x1+z1 is 6.0, the ...
PUM
| Property | Measurement | Unit |
|---|---|---|
| thickness | aaaaa | aaaaa |
| melting point | aaaaa | aaaaa |
| thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 