Silver chloride-titanium dioxide nanotube composite material and preparation method and application thereof
A technology of titanium dioxide and composite materials, applied in chemical instruments and methods, special compound water treatment, physical/chemical process catalysts, etc., can solve cumbersome, complicated methods, time-consuming and labor-intensive problems
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0024] The present invention also provides a preparation method of silver chloride-titanium dioxide nanotube composite material, comprising:
[0025] Step 1: Mix and stir titanium dioxide P25 and NaOH solution, the stirring time is preferably 30-60min to obtain a mixed solution; the mass (g) of titanium dioxide P25: NaOH solution (ml) is preferably (0.6-1.0): (30-50); the concentration of NaOH solution is preferably 10mol L -1 ;
[0026] Step 2: Put the mixed solution obtained in Step 1 into a reactor, which is preferably a polytetrafluoroethylene-lined reactor, and then raise the temperature from room temperature to 130-150°C at a rate of 2°C / min. And keep it for 24 hours to obtain the mixture; the mixture is acid-washed, preferably: the cooled mixture is taken out, washed repeatedly with distilled water until the pH value is 6.8-7.2, and then washed with 0.1mol·L -1 Wash with HCl solution until the pH value is 1.0, ultrasonication for 30-60min, and standing for 3-5h;
[0...
Embodiment 1
[0033] Mix 0.6gP25 with 30ml of 10mol·L -1 The NaOH solution was mixed and stirred for 60 minutes, then the mixed solution was transferred into a polytetrafluoroethylene-lined reaction kettle, placed in a temperature-programmed oven, and the temperature was raised from room temperature to 150°C at a rate of 2°C / min, and kept for 24h. The final mixture was taken out, washed repeatedly with distilled water until the pH value was about 7.0, and then washed with 0.1mol·L -1 The HCl solution was washed until the pH value was about 1.0, after ultrasonication for 30min, and after standing for 3h, 0.007g, 0.0373g and 0.079g of AgNO were added to the mixture 3 , the mixture was washed again with pure water until the pH value was about 7.0, and then dried in an oven at 80°C for 12h, and the dried solid was placed in a muffle furnace and calcined at 400°C for 2h to obtain an AgCl content of 1%. , 5% and 10% silver chloride-titanium dioxide nanotube composites.
Embodiment 2
[0035] Mix 0.8g P25 with 40ml of 10mol·L -1 The NaOH solution was mixed and stirred for 45 minutes, then the mixed solution was transferred into a polytetrafluoroethylene-lined reactor, placed in a temperature-programmed oven, and the temperature was raised from room temperature to 140°C at a rate of 2°C / min, and kept for 48h. The final mixture was taken out, washed repeatedly with distilled water until the pH value was about 6.8, and then washed with 0.1mol·L -1 HCl solution was washed until the pH value was about 1.0, after ultrasonication for 30min, and after standing for 3h, 0.01g of AgNO was added to the mixture 3, the mixture was washed again with pure water until the pH value was about 7.0, and then dried in an oven at 100°C for 12h, and the dried solid was placed in a muffle furnace and calcined at 400°C for 2h to obtain silver chloride-titanium dioxide nanotube composites. The physical and chemical properties of the AgCl / TNTs surface obtained in Example 2 are: avera...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More - R&D
- Intellectual Property
- Life Sciences
- Materials
- Tech Scout
- Unparalleled Data Quality
- Higher Quality Content
- 60% Fewer Hallucinations
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com