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Heat-treatment technology of high-plasticity nickel base alloy

A nickel-based alloy, high plasticity technology, applied in the field of heat treatment of high-plasticity nickel-based alloys, can solve the problems of increased alloy elongation, increased section shrinkage, poor alloy plasticity, etc., to reduce process time, increase strength, and improve The effect of production efficiency

Active Publication Date: 2016-08-03
SINO EURO MATERIALS TECH OF XIAN CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In order to overcome the above-mentioned deficiencies in the prior art, the purpose of the present invention is to provide a heat treatment process for high-plasticity nickel-base alloys, which solves the shortcoming of poor plasticity of Ni-Co-Cr type nickel-base powder alloys, compared with existing data , can increase the elongation of the alloy by 35-40%, and the reduction of area by 30-35%; the present invention does not affect the strength of the alloy; compared with the traditional process, the improved heat treatment system is often shortened from 43 hours to 25 hours, Reduced cost, more suitable for industrial production

Method used

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  • Heat-treatment technology of high-plasticity nickel base alloy
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  • Heat-treatment technology of high-plasticity nickel base alloy

Examples

Experimental program
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Effect test

Embodiment 1

[0029] In this example, 1) The nickel-based powder alloy was prepared according to the following mass percentages: Co: 15.3%, Cr: 9.4%, Al: 4.7%, Ti: 1.8%, W: 5.2%, Mo: 4.1%, C: 0.43 %, Nb: 2.6, Hf: 0.23%, B: 0.010, Ni balance;

[0030] 2) The above-mentioned nickel-based powder alloy is treated by solid solution and aging process, and is subjected to vacuum induction melting and electroslag remelting to obtain 800*Ф80 bar with surface roughness Ra <1.6, use PREP powder milling equipment to process metal powder, put it into the sheath, and perform hot isostatic pressing;

[0031] 3) The hot isostatic pressing alloy tape sheath obtained in step 2) is heat treated, solution treated at 1040°C, kept in a muffle furnace for 2 hours, then taken out and cooled to room temperature in air, and then at 780°C The aging time is 8 hours; then the temperature is reduced to 680°C at a rate of 0.6°C / min, and the heat preservation is 8 hours. The entire heat treatment time is 22 hours. Table 3 sho...

Embodiment 2

[0033] In this embodiment, 1) The nickel-based powder alloy is prepared according to the following mass percentages: Co: 15.4%, Cr: 9.6%, Al: 4.8%, Ti: 1.7%, W: 5.5%, Mo: 3.8%, C: 0.36 %, Nb: 2.5, Hf: 0.26%, B: 0.008, Ni balance;

[0034] 2) The above-mentioned nickel-based powder alloy is subjected to vacuum induction melting and electroslag remelting to obtain a 700*Ф70 bar with a surface roughness of Ra <1.6, use PREP powder milling equipment to process into metal powder, and then put it into the sheath for hot isostatic pressing;

[0035] 3) The nickel-based powder alloy hot isostatically pressed in step 2) is subjected to heat treatment, solution treatment at 1060°C, and heat preservation in a muffle furnace for 5 hours, after which it is taken out and air-cooled to room temperature. , Aging at 750°C, the aging time is 7 hours; then the temperature is reduced to 610°C at a rate of 0.3°C / min, and the heat preservation is 7 hours. The entire heat treatment time is 25 hours. Tab...

Embodiment 3

[0037] In this example, 1) The nickel-based powder alloy was prepared according to the following mass percentages: Co: 15.6%, Cr: 9.1%, Al: 4.9%, Ti: 1.8%, W: 5.3%, Mo: 3.8%, C: 0.35 %, Nb: 2.5, Hf: 0.22%, B: 0.011, Ni balance;

[0038] 2) The above-mentioned nickel-based powder alloy is treated by solid solution and aging process, and is subjected to vacuum induction melting and electroslag remelting to obtain 800*Ф80 bar with surface roughness Ra <1.6, use PREP powder milling equipment to process into metal powder, and then put it into the sheath for hot isostatic pressing;

[0039] 3) The hot isostatic pressing alloy tape sheath obtained in step 2) is heat-treated, solution-treated at 1070°C, kept in a muffle furnace for 1 hour, then taken out and air-cooled to room temperature, and then at 800°C The aging time is 8 hours; then the temperature is reduced to 680°C at a rate of 1°C / min, and the heat preservation is 8 hours. The entire heat treatment time is 21 hours.

[0040] Table...

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PUM

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Abstract

A heat-treatment technology of a high-plasticity nickel base alloy comprises following steps: firstly, the temperature of the alloy rises, then, low-temperature solid-solution treatment is carried out, and after the alloy keeps warm for a certain period, air cooling is carried out; two-stage low-temperature aging is carried out; and the technical problems that the alloy is poor in plasticity and too long in heat treatment duration are solved. The strength of the alloy prepared through the method is slightly improved, the plasticity is obviously improved, the rising amplitude reaches 30 % to 35%, the heat treatment duration is one half of the original heat treatment duration, and the heat treatment time is greatly shortened.

Description

Technical field [0001] The invention relates to a heat treatment process of a high-plasticity nickel-based alloy. Background technique [0002] Nickel-based alloys have a series of advantages such as high service temperature, high creep performance, high durability, high resistance to high temperature oxidation, etc., and are widely used in aero engines, gas turbines and other fields. Nickel-based powder alloy is a new type of alloy. Compared with traditional casting and forging alloys, it has a series of advantages such as no macrosegregation, fine grain, uniform structure, and low cost. It can also produce some alloys with poor hot workability. At present, it has become a required material for key hot-end components of aerospace engines. Well-known institutions and companies, including NASA, GE, P&W, Rolls-Royce, etc., are developing advanced powder superalloys. At present, the most advanced military and civil aircraft in the world, such as A320, A330, B777, B787, F35, etc., w...

Claims

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Application Information

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IPC IPC(8): C22F1/10C22C19/05C22C1/04
CPCC22C1/0433C22C19/056C22F1/10
Inventor 闫飞王庆相韩志宇梁书锦张平祥左振博相敏王琦莫茗锟
Owner SINO EURO MATERIALS TECH OF XIAN CO LTD