A system and method for continuously preparing organic-inorganic nano-hybrid coatings
An inorganic nano and hybrid technology, applied in chemical instruments and methods, coatings, mixers, etc., can solve problems such as poor batch stability, high process energy consumption, and low process efficiency, and achieve good batch stability, The effect of high coating hardness and high production efficiency
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Embodiment 1
[0039] Such as figure 1 As shown, this embodiment provides a system for continuously preparing organic-inorganic nano-hybrid coatings. The system includes a first premixing kettle 1, a second premixing kettle 4, a concentration kettle 5, a raw material storage tank 8, and a finished product storage tank. Tank 9, first feed pump 2, second feed pump 3, third feed pump 6, fourth feed pump 7, static mixer 10, ultrasonic enhanced tubular reactor 11, liquid atomizer 12, Vacuum device 13 and ultrasonic intensified static mixer 14; Wherein the first premixing kettle 1 and the second premixing kettle 4 are respectively connected with two inlets of the static mixer 10 through the first feeding pump 2 and the second feeding pump 3 , the raw material storage tank 8 and the concentration kettle 5 are respectively connected to the two inlets of the ultrasonically enhanced static mixer 14 through the third feeding pump 6 and the fourth feeding pump 7, and the outlet of the static mixer 10 is...
Embodiment 2
[0050] Such as figure 2 As shown, this embodiment provides a system for continuously preparing organic-inorganic nano-hybrid coatings. The system includes a first pre-mixing tank 1, a second pre-mixing tank 4, a raw material storage tank 8, a finished product storage tank 9, and a first pre-mixing tank. A feeding pump 2, a second feeding pump 3, a third feeding pump 6, a static mixer 10, an ultrasonically enhanced tubular reactor 11, and an ultrasonically enhanced static mixer 14; wherein the first premix tank 1 and the first The premix tank 4 is connected to the two inlets of the static mixer 10 through the first feeding pump 2 and the second feeding pump 3 respectively, and the outlet of the static mixer 10 is connected to the inlet of the ultrasonically enhanced tubular reactor 11, and the ultrasonically enhanced The outlet of the tubular reactor 11 is connected with an inlet of the ultrasonically enhanced static mixer 14, and the raw material storage tank 8 is connected w...
Embodiment 3
[0059] The system for continuously preparing organic-inorganic nano-hybrid coatings provided by Example 1 is used to rapidly prepare high-hardness water-based coatings, including the following steps:
[0060] (1) 1000 grams of water-based alumina sol with a solid content of 15 wt % and an average particle size of nano-alumina of 80 nm and 1 gram of Tween 80 were added to the first premixing kettle 1 and mixed evenly, and the material temperature was maintained at 70 ° C.
[0061] (2) Add 10 grams of 3-methacryloxypropyltrimethoxysilane, 300 grams of water and 1 gram of sodium lauryl sulfate into the second pre-mixing tank 4 and mix well.
[0062] (3) Turn on the ultrasonic wave in the ultrasonic intensified tubular reactor in advance.
[0063] (4) Utilize the first feed pump 2 and the second feed pump 3 to input the material in the first premix kettle 1 and the second premix kettle 4 in the static mixer 10 to realize the rapid mixing of the materials respectively, The materia...
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Abstract
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