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Preparation method and application of novel CpGISS vaccine adjuvant

A vaccine adjuvant and a new technology, applied in the field of preparation of new CpGISS vaccine adjuvants, can solve the problems that CpG preparations are difficult to enter cells, easily degraded by nucleases, and lose activity, so as to improve the survival rate and immune protection rate. The level of cellular immune response, the effect of rapid replication

Pending Publication Date: 2017-09-08
浙江皇冠科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The preparation of CpG ISS by this method is artificially synthesized, which has high cost and low efficiency; the prepared CpG preparation is difficult to enter cells and is easily degraded by nucleases, thereby losing activity

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of a novel CpGISS vaccine adjuvant, the preparation steps are:

[0020] 1) After the activation culture, primary shake flask culture and secondary shake flask culture are performed on the preserved Pichia pastoris, the strain is inoculated into a sterilized fermenter. The components of the fermentation medium and their parts by weight are: 50-60 parts of sucrose, 60-80 parts of yeast powder, 10-15 parts of peptone, 30-45 parts of urea, 6-9 parts of wort juice, KH 2 PO 4 8~12 copies, K 2 HPO 4 ·3H 2 O 5~7 parts, MgSO 4 ·7H 2 O 0.2~0.3 parts, ZnSO 4 ·7H 2 O 5~7.8 parts, MnSO 4 4H 2 O 24~35 parts, biotin 0.016~0.02 parts, riboflavin sodium phosphate 0.003~0.005 parts, eicosapentaenoic acid ethyl ester 0.02~0.06 parts and deionized water 1700~2000 parts. Adjust the rotation speed and air flow, and control the dissolved oxygen content in the culture medium to 30-38%. During the fermentation process, the pH of the culture medium is controlled b...

Embodiment 2

[0025] A kind of preparation method of novel CpGISS vaccine adjuvant, the most preferred steps are:

[0026] 1) After the activation culture, primary shake flask culture and secondary shake flask culture are performed on the preserved Pichia pastoris, the strain is inoculated into a sterilized fermenter. The components of the fermentation medium and the most preferred parts by weight are: 56 parts of sucrose, 72 parts of yeast powder, 13 parts of peptone, 40 parts of urea, 8 parts of wort, KH 2 PO 4 10 copies, K 2 HPO 4 ·3H 2 O 6 parts, MgSO 4 ·7H 2 O 0.25 parts, ZnSO 4 ·7H 2 O 7.2 parts, MnSO 4 4H 2 33 parts of O, 0.019 parts of biotin, 0.005 parts of riboflavin sodium phosphate, 0.04 parts of ethyl eicosapentaenoate and 1800 parts of deionized water. Adjust the rotation speed and air flow rate, and control the dissolved oxygen content in the culture medium to 36%. During the fermentation process, the pH of the culture medium is controlled to be 5.0 by adding ammon...

Embodiment 3

[0031] A preparation method of a novel CpGISS vaccine adjuvant, the preparation steps are:

[0032] 1) After the activation culture, primary shake flask culture and secondary shake flask culture are performed on the preserved Pichia pastoris, the strain is inoculated into a sterilized fermenter. The components of the fermentation medium and their parts by weight are: 54 parts of sucrose, 72 parts of yeast powder, 13 parts of peptone, 41 parts of urea, 7 parts of wort, KH 2 PO 4 10 copies, K 2 HPO 4 ·3H 2 O6 parts, MgSO 4 ·7H 2 O 0.2 parts, ZnSO 4 ·7H 2 O 6.5 parts, MnSO 4 4H 2 30 parts of O, 0.017 parts of biotin, 0.003 parts of riboflavin sodium phosphate, 0.04 parts of ethyl eicosapentaenoate and 1800 parts of deionized water. Adjust the rotating speed and air flow, and control the dissolved oxygen content in the culture medium to 35%. During the fermentation process, the pH of the culture medium is controlled to be 5.0 by adding ammonia water, and the culture tem...

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Abstract

The invention discloses a preparation method and application of a novel CpGISS vaccine adjuvant. A large number of CpGISS is produced by adopting a fermentation method, and gold nanoparticles are adopted as carriers for adsorption, so as to obtain the novel CpGISS vaccine adjuvant. The preparation method has the beneficial effects that a fermental culture medium is adopted for fermental culture, so that the multiplication speed of pichia pastoris is high, the unwinding and replication rate of the unmethylated CpGISS are high, and the yield of the CpGISS is high; a large number of CpGISS is produced by adopting a fermentation manner, so that the cost is low, and the safety is high; CpGISS-gold nanoparticles compounds enter into cells extremely easily, and the biological function of the CpGISS is not influenced; through the use of the vaccine adjuvant, the immunity period can be shortened, and the immunity effect is good; when the vaccine adjuvant is used in animal breeding and production or human bodies, the survival rate and the immune protection rate are improved.

Description

technical field [0001] The invention relates to the technical field of vaccine adjuvant preparation, in particular to a preparation method and application of a novel CpGISS vaccine adjuvant. Background technique [0002] Vaccine adjuvants of many vaccine manufacturers in China use aluminum adjuvants or oil adjuvants, but this type of adjuvant has certain side effects. Oil emulsion stimulates local granuloma or inflammation: aluminum adjuvant can cause local inflammation at the injection site The reaction in turn causes granulomas, and some individuals cause stress reactions in the injected subjects and lead to the death of individual individuals. And the induced immune response belongs to Th2 type, which is not enough to completely protect animals against infection. Although it can enhance humoral immunity, the antibody is mainly IgGⅠ, which cannot significantly improve cell-mediated immune response, cannot enhance cellular immunity, and has limitations; it may also cause d...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K39/39C12P19/36C12R1/84
CPCA61K39/39A61K2039/55561C12P19/36
Inventor 胡向东叶茂梁新乐邵建忠
Owner 浙江皇冠科技有限公司