Epoxy Resin Composition for Die Bonding
An epoxy resin and chip bonding technology, applied in the direction of epoxy resin glue, novolac epoxy resin adhesive, adhesive type, etc., can solve the problems of low adhesion, high surface viscosity, unfavorable operation, etc. , to achieve the effect of convenient operation and high adhesive strength
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Embodiment 1 and comparative example 1 and 2
[0049] Example 1 and Comparative Examples 1 and 2: Preparation of epoxy resin composition for die bonding
[0050] The components were mixed with the composition shown in Table 1 below to prepare an epoxy resin composition for die bonding (unit: wt%).
[0051] [Table 1]
[0052]
[0053] 1) Hypro 1300X13NA CTBN (CVC thermoset specialties)
[0054] 2) B-Tough A3(Croda)
[0055] 3)EOCN-1020(Nippon kayaku)
[0056] 4) YDCN-500-4P (Kukdo Chemical)
[0057] 5) CNE80208(KCC)
[0058] 6) MEH-7800SS(Meiwa)
[0059] 7) DICY (Air product)
[0060] 8) Carbitol Acetate (Samchun Chemical)
[0061] 9) AEROSIL R 972(EVONIK)
[0062] 10) SFP-30M (Denka)
[0063] 11) EP-2601(Dow corning)
[0064] 12) IXEPLAS-A1(Toagosei)
[0065] 13) IXE-600(Toagosei)
[0066] 14) LC550(SHIN-A T&C)
[0067] 15) BYK110(BYK Additive&Instruments)
[0068] 16) BYK-085(BYK Additive&Instruments)
[0069] 17) BYK-A501(BYK Additive&Instruments)
[0070] 18) S-510(CHISSO)
experiment example 1
[0072] The physical properties of the epoxy resin compositions prepared in Example 1 and Comparative Examples 1 and 2 were measured by the following methods, and the results are shown in Table 2 below.
[0073] (1) Viscosity and thixotropy index
[0074] Take a sample of about 0.5 ml of the composition, and measure the viscosity at 25° C. at a rotation speed of 0.5 rpm and 25 rpm in a Brookfield cone / plate viscometer using a rotor CP-51. The value measured at 5 rpm was taken as the viscosity value, and the thixotropic index was calculated as the ratio of the two viscosity values measured at 0.5 rpm and 5 rpm, that is, the value measured at 0.5 rpm / the value measured at 5 rpm.
[0075] (2) Glass transition temperature (Tg) and elastic modulus
[0076] A sample of the composition was coated in a thickness of 0.2 mm and cured at 125° C. / 30 minutes and 175° C. / 120 minutes, and then measured in a tensile mode using Perkin ELmer DMA 8000.
[0077] (3) Laboratory shear strength
[0078] Acco...
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