Coating agent and method of forming a coating layer using thereof
A coating and coating technology, applied in the direction of coating, device for coating liquid on the surface, temporary coating, etc., can solve the problem of difficult to apply semiconductor wafer processing technology, laminated film can not be uniformly bonded, easy to damage surface protection film and other problems, to achieve the effect of less variation, excellent flatness and low price
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Embodiment 1
[0126] A composition (1) consisting of 65% by weight of polyvinyl chloride slurry resin (EL103 of Hanwha Petrochemical) and 35% by weight of trioctyl trimellitate (TOTM) having Newtonian fluid characteristics was discharged using a quantitative discharge pump. It is discharged to the surface of the semiconductor wafer, and then the upper plate in the mold is pulled down, and the 2 After performing thermocompression bonding, heat treatment was performed at 150° C. for 10 minutes, and then, after the pressing was released, the formed film was removed with a remover. At this time, as the polyvinyl chloride slurry resin, a polyvinyl chloride resin having an average particle diameter of 2.98 μm, a degree of polymerization of 900, and a viscosity of 20,000 cps at 30° C. was used.
Embodiment 2
[0128] For the mixture of 65% by weight of polyvinyl chloride slurry resin and 35% by weight of trioctyl trimellitate (TOTM) with Newtonian fluid properties, in 100 parts by weight of the mixture, mix 1.0, 0.5, 0.4 The leveling agent of weight part is the EX-570 of Troy Company, the defoamer is the Foamstar A-10 of Corning Company, the viscosity modifier is hydroxymethyl cellulose, forms composition (2), and utilizes quantitative discharge pump to Composition (2) is discharged on the surface of the semiconductor wafer, and then the upper plate in the mold is pulled down, and at 150 ° C at 25TONf / cm 2 After performing thermocompression bonding, heat treatment was performed at 150° C. for 10 minutes, and then, the formed film was removed with a remover after the pressing was released.
Embodiment 3
[0130] For the mixture of 65% by weight of polyvinyl chloride slurry resin and 35% by weight of trioctyl trimellitate (TOTM) with Newtonian fluid properties, in 100 parts by weight of the mixture, mix 1.0, 0.5, 4.0 , 0.5, 1.0 and 2.0 parts by weight of the leveling agent is the EX-570 of Troy Company, the defoamer is the Foamstar A-10 of the Corning Company, the viscosity modifier is hydroxymethyl cellulose, and the anti-sedimentation agent is the BYK company BYK-405, heat stabilizer is BZ-806P of Song Yuan Industry, antistatic agent is polyvinyl alcohol 800 (PEG800) of Lotte Chemical to form composition (3), and use quantitative discharge pump to discharge composition (3) on the surface of the semiconductor wafer, then the upper plate inside the mold is pulled down, and at 150°C at 25TONf / cm 2 After performing thermocompression bonding, heat treatment was performed at 150° C. for 10 minutes, and then, the formed film was removed with a remover after the pressing was released....
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