A kind of preparation method of curing agent for medium and high temperature damping polyurethane
A polyurethane, medium and high temperature technology, applied in the field of preparation of curing agent for medium and high temperature damping polyurethane, can solve the problems of large damping factor change, low glass transition temperature, unfavorable use, etc., to increase the glass transition temperature and broaden the damping Temperature range, the effect of increasing frictional resistance
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Embodiment 1
[0028] (1) Dehydration treatment of TDI, diazobisphenol fluorene and trimethylolpropane (dehydration treatment with 5A molecular sieves), and set aside;
[0029] (2) Take 31 parts by weight of dehydrated diisocyanate and 41 parts by weight of xylene in N 2 Add to a dry three-necked flask and mix under atmosphere, stir and heat up to 30°C;
[0030] (3) Dissolve 0.5 parts by weight of dehydration-treated diazobisphenol fluorene and 7.5 parts by weight of dehydration-treated trimethylolpropane in 20 parts by weight of DMF, and add the resulting mixture dropwise to the step through a constant pressure funnel. (2) In the three-necked flask, the temperature was raised to 70°C, and the temperature was kept for 1.5 hours;
[0031] (4) Take a sample of the reaction product in step (3), use the acetone-di-n-butylamine method to detect its NCO content, calculate and titrate the NCO content until it is close to the theoretical value, and then discharge the product, and test the NCO conte...
Embodiment 2
[0033] (1) Dehydration treatment of IPDI, diazobisphenol fluorene and trimethylolpropane (dehydration treatment with 5A molecular sieves), and set aside;
[0034] (2) Take 31 parts by weight of dehydrated diisocyanate and 41 parts by weight of butyl acetate in N 2 Add to a dry three-necked flask and mix under atmosphere, stir and heat up to 50°C;
[0035] (3) Dissolve 1 part by weight of dehydration-treated diazobisphenol fluorene and 7 parts by weight of dehydration-treated trimethylolpropane in 20 parts by weight of cyclohexanone, and add the resulting mixture dropwise through a constant pressure funnel into the three-neck flask described in step (2), then raise the temperature to 90°C, and keep the temperature for 1.5h;
[0036] (4) Take a sample of the reaction product in step (3), use the toluene-di-n-butylamine method to detect its NCO content, calculate and titrate the NCO content until it is close to the theoretical value, and then discharge the product, and test the ...
Embodiment 3
[0038] (1) Dehydrate MDI, diazobisphenol fluorene, and trimethylolpropane (dry in vacuum at 60°C), and set aside;
[0039] (2) Take 31 parts by weight of dehydrated diisocyanate and 41 parts by weight of acetone in N 2 Add to a dry three-necked flask and mix under atmosphere, stir and heat up to 40°C;
[0040] (3) Dissolve 1.5 parts by weight of dehydration-treated diazobisphenol fluorene and 6.5 parts by weight of dehydration-treated trimethylolpropane in 20 parts by weight of DMSO, and add the resulting mixture dropwise to the step through a constant pressure funnel. (2) In the three-necked flask, the temperature was raised to 80°C, and the temperature was kept for 1.5 hours;
[0041] (4) Take a sample of the reaction product in step (3), use the N,N-dimethylformamide-di-n-butylamine method to detect its NCO content, calculate and titrate the NCO content, discharge until it is close to the theoretical value, and test again For the NCO content of the product, the product wa...
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