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Tricyclazole water suspending agent composition

A technology of suspending agent and composition, applied in the field of pesticides, can solve the problems of reducing the advantages of wettable powder and granule products, the aggregation and growth of small particles, and the crystallization of products, achieving unique steric hindrance effects and solving the problem of stable storage The effect of poor performance and smooth grinding process

Inactive Publication Date: 2017-12-22
江苏长青生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, since the solubility of tricyclazole in water has reached 1.6g / L, it is a species with relatively high solubility in water. The processed suspension product will undergo Ostwald aging during storage, resulting in the crystallization of the product. The small particles aggregate and grow, and the particle size becomes larger, resulting in a decrease in drug efficacy. Products with high content of suspending agent may even be unusable due to the hardening of the material due to Austenitic ripening.
Therefore, the suspending agent products in the current market are mostly products with low content of 20~30%, and its content determines its large dosage and high packaging and transportation costs, which also reduces its advantages over wettable powder and granule products.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0013] 40% tricyclazole suspension concentrate

[0014] Tricyclazole original drug (97.5%)

410 grams

ATLAX G5002LQ®

12 grams

SPED-27001®

28 grams

Antifreeze Propylene Glycol

30 grams

Preservative Cathone

1.0g

Silicone defoamer

1.5 grams

Crystallization Inhibitor PVP K30

3.0 grams

thickener xanthan gum

1.2 grams

Deionized water

Make up 1000 grams

[0015] Add 1.2 grams of xanthan gum and 30 grams of propylene glycol into a 200 ml beaker, stir well to make the xanthan gum fully wetted by propylene glycol, then add 6, 7.8 grams of deionized water, 1.0 grams of Casson, and stir well to make the yellow The original gum is completely dispersed in water, and placed in a refrigerator at about 0 degrees for more than 24 hours to make the xanthan gum fully swell, and after stirring evenly, 100 grams of xanthan gum aqueous solution is formed for later use.

[0016] Add 410 grams of tr...

example 2

[0018] 50% tricyclazole suspension concentrate

[0019] Tricyclazole original drug (97.5%)

513 grams

ATLAX G5002LQ®

15 grams

SPED-27001®

35 grams

Antifreeze Propylene Glycol

30 grams

Preservative Cathone

1.0g

Silicone defoamer

1.5 grams

Crystallization Inhibitor PVP K60

5.0 grams

thickener xanthan gum

1.0g

Deionized water

Make up 1000 grams

[0020] Add 1.0 grams of xanthan gum and 30 grams of propylene glycol into a 200 ml beaker, stir well to make the xanthan gum fully wetted by propylene glycol, then add 68 grams of deionized water, 1.0 grams of Casson, and stir well to make the xanthan gum Completely disperse in water, place in a refrigerator at about 0 degrees for more than 24 hours to make the xanthan gum fully swell, stir well and form 100 grams of xanthan gum aqueous solution for later use.

[0021] Add 513 grams of tricyclazole original drug to a 2000ml vertical sm...

example 3

[0023] 60% tricyclazole suspension concentrate

[0024] Tricyclazole original drug (97.5%)

616 grams

ATLAX G5002LQ®

20 grams

SPED-27001®

40 grams

Antifreeze Propylene Glycol

30 grams

Preservative Cathone

1.0g

Silicone defoamer

1.5 grams

Crystallization Inhibitor PVP K90

10.0 grams

thickener xanthan gum

0.8 grams

Deionized water

Make up 1000 grams

[0025] Add 0.8 grams of xanthan gum and 30 grams of propylene glycol into a 200 ml beaker, stir well to make the xanthan gum fully wetted by propylene glycol, then add 68.2 grams of deionized water, 1.0 grams of Casson, and stir well to make the xanthan gum Completely disperse in water, place in a refrigerator at about 0 degrees for more than 24 hours to make the xanthan gum fully swell, stir well and form 100 grams of xanthan gum aqueous solution for later use.

[0026] Add 615 grams of tricyclazole original drug to a 2000ml ver...

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PUM

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Abstract

The invention relates to tricyclazole water suspending agent composition. The tricyclazole water suspending agent composition is prepared from, by mass percent, 40-70 parts of tricyclazole active compound, 2-10% of wetting dispersant, 0.3-1.0% of crystallization inhibitor, and allowance of deionized water. The tricyclazole water suspending agent composition can effectively solve the technical difficulty of ostwald ripening existed in the high-content suspending agent proceed by tricyclazole active compound, and a problem of poor storage stability of the water suspending agent product with high content of tricyclazole. Meanwhile, the formula also can solve the problems of big viscosity, poor mobility, low processing efficiency, and others caused by high solid content of the product when the high-content suspending agent product is processed.

Description

technical field [0001] The invention relates to a tricyclazole water suspension composition and belongs to the technical field of pesticides. Background technique [0002] Tricyclazole, also known as clemenazole, clemenazole, biyan, and rice blastazole, is a protective triazole fungicide with strong systemic properties. It has special effects in preventing and treating rice blast. The roots, stems, and leaves of rice can absorb it and transport it in the plant. Spraying it once or twice during the entire growth period of rice can effectively prevent the occurrence of rice blast. Tricyclazole has strong anti-scouring ability, and it does not need to be re-sprayed in case of rain after 1 hour of spraying. It mainly inhibits spore germination and episporium formation, thereby effectively preventing the invasion of pathogens and reducing the production of spores of Magnaporthe grisea. Tricyclazole has strong systemic and transport properties, and it decomposes slowly in the pl...

Claims

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Application Information

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IPC IPC(8): A01N43/90A01N25/04A01N25/30A01P3/00
CPCA01N25/04A01N25/30A01N43/90
Inventor 于国权孙霞林陈素云丁华平
Owner 江苏长青生物科技有限公司
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