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One-component boiled glue and preparation method thereof

A one-component, boiled technology, applied in the direction of adhesives, non-polymer adhesive additives, adhesive types, etc. high viscosity problem

Active Publication Date: 2020-07-07
GUANGZHOU SHUANGKE NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Epoxy AB glue has a high viscosity, which is not conducive to glue application. After the cutting is completed, it takes a long time for the crystal holder to separate from the glass, and the smell is strong

Method used

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  • One-component boiled glue and preparation method thereof
  • One-component boiled glue and preparation method thereof
  • One-component boiled glue and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] In this embodiment, a one-component boiled gelatin comprises the following components in parts by weight:

[0030] 15 parts of triethylene glycol dimethacrylate, 20 parts of tetrahydrofurfuryl acrylate, 15 parts of hydroxyethyl methacrylate, 15 parts of two-functional polyurethane acrylate (Sartomer CN8881NS), cumene 4 parts of hydrogen peroxide, 0.5 parts of saccharin, 0.05 parts of p-benzoquinone, 1 part of fumed silica, 20 parts of azodicarbonamide, 10 parts of urea fat BK.

[0031] The preparation method of the above-mentioned one-component boiled gelatin comprises the following steps:

[0032] Step 1, weigh triethylene glycol dimethacrylate, tetrahydrofurfuryl acrylate, hydroxyethyl methacrylate, difunctional polyurethane acrylate, saccharin, p-benzoquinone, gas phase dioxide Add silicon, azodicarbonamide, and urea fat BK into the reaction kettle, raise the temperature to 40°C, and stir for 2 hours at a speed of 600r / min;

[0033] Step 2, after the reaction is fi...

Embodiment 2

[0041] In this embodiment, a one-component boiled gelatin comprises the following components in parts by weight:

[0042] 12 parts of triethylene glycol dimethacrylate, 24 parts of tetrahydrofurfuryl acrylate, 17 parts of hydroxyethyl methacrylate, 12 parts of difunctional polyurethane acrylate (Sartomer CN966J75NS), cumene 5 parts of hydrogen peroxide, 0.7 parts of saccharin, 0.07 parts of p-benzoquinone, 1 part of fumed silica, 21 parts of azodicarbonamide, and 8 parts of urea fat BK.

[0043] The preparation method and construction process of the one-component boiled glue in Example 2 are the same as in Example 1.

Embodiment 3

[0045] In this embodiment, a one-component boiled gelatin comprises the following components in parts by weight:

[0046] 14 parts of triethylene glycol dimethacrylate, 18 parts of tetrahydrofurfuryl acrylate, 18 parts of hydroxyethyl methacrylate, 15 parts of two-functional polyurethane acrylate (Changxing 6148J75), cumene peroxidation 5 parts of hydrogen, 0.7 parts of saccharin, 0.07 parts of p-benzoquinone, 1 part of fumed silica, 16 parts of azodicarbonamide, and 13 parts of urea fat BK.

[0047] The preparation method and construction process of the one-component boiled glue in Example 3 are the same as in Example 1.

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Abstract

The invention relates to single component poached glue and a preparation method thereof. The single component poached glue is prepared from the following components in parts by weight: 12-18 parts of triethylene-glycol dimethacrylate, 16-24 parts of tetrahydrofurfuryl acrylate, 12-18 parts of hydroxyethyl methylacrylate, 12-18 parts of polyurethane acrylate, 3-5 parts of an initiator, 0.3-0.7 part of an accelerant, 0.03-0.07 part of a polymerization inhibitor, 0.5-1.5 parts of a thixotropic agent, 16-24 parts of azodicarbonamide and 7-13 parts of urea grease BK. The single component poached glue has good storage stability, and the storage period reaches more than 1 year; the single component poached glue is high in curing efficiency and high in adhesive force, and can be quickly poached to unglue, so that the production efficiency of a silicon wafer can be increased greatly.

Description

technical field [0001] The invention relates to the field of adhesives, in particular to a single-component boiled glue and a preparation method thereof. Background technique [0002] As an important semiconductor material, silicon has good electrical properties and thermal stability. Since it was discovered and utilized by people in the 1960s, it has rapidly replaced single crystal germanium as the main material of semiconductors. Compared with other semiconductor materials, silicon single crystal has the characteristics of high hardness and rich source of raw materials, and has the advantages of easy growth of large-sized high-purity crystals, excellent thermal and mechanical properties, and so on. [0003] Wafer cutting is an upstream key technology for the production of silicon wafers (wafers), the main raw material in the electronics industry. The quality and scale of cutting directly affect the subsequent production of the entire industrial chain. In the electronics i...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09J175/14C09J11/06C09J11/04
CPCC08K3/36C08K5/08C08K5/21C09J11/04C09J11/06C09J175/14
Inventor 梁锦坤韦士应温科雄肖世荣
Owner GUANGZHOU SHUANGKE NEW MATERIAL