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A purification method for waste lubricating oil classification and impurity removal

A technology of waste lubricating oil and oil products, which is applied in the direction of lubricating compositions, etc., can solve the problems of adsorption and excessive consumption, accelerated asphalt detachment, poor quality of recycled oil products, etc., and achieve the effect of simple process, strong operability and high quality

Active Publication Date: 2020-07-28
麻城天安化工股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to solve the problems such as difficult removal of impurities such as asphalt and colloid, large amount of adsorption and consumption, and poor quality of regenerated oil in the regeneration process of existing waste lubricating oil, and provide a purification method for waste lubricating oil classification and impurity removal, This method uses organic solvents, heating and electrolytes to accelerate the separation of asphalt and colloids from oil products, and cooperates with alkaline particles with a certain porosity to further remove residual colloids and acidic impurities. The magnetic particles separate the metal impurities, and finally the carbon and silicon filter layer is used to effectively remove the carbon and particle impurities in the oil. Through the above treatment, high-quality purified oil can be obtained, and its index even reaches the standard of lubricating base oil

Method used

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  • A purification method for waste lubricating oil classification and impurity removal
  • A purification method for waste lubricating oil classification and impurity removal
  • A purification method for waste lubricating oil classification and impurity removal

Examples

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Embodiment 1

[0021] Using waste lubricating oil from small cars as raw material, heat the waste lubricating oil to 80°C through the dilution and degumming process, add n-heptane at a ratio of 1:0.5 to the volume of the oil agent, and then add CaCl2 equivalent to 5% of the mass of the waste lubricating oil, Stir for 15 minutes, centrifuge to remove gum and asphalt. Add alkalized particles with a particle size of 60-100 mesh to the upper-stage filtrate through the alkalization degumming acid process at a liquid-solid volume ratio of 1:0.1, stir rapidly for 5 minutes, and then centrifugally filter. Add 50-100-mesh high-strength magnetic particles to the upper-stage filtrate at a liquid-solid volume ratio of 1:0.3 through the magnetic desquamation process, stir rapidly for 5 minutes, and centrifugally filter. Through the carbon silica gel decolorization process, the upper-stage filtrate is filtered through a 1-10um activated carbon silica gel layer to obtain solvent-containing purified oil. Fi...

Embodiment 2

[0026] Using waste lubricating oil from motor vehicles as raw material, heat the waste lubricating oil to 50°C through the dilution and degumming process, add n-heptane at a ratio of 1:1.2 to the volume of the oil agent, and then add CaCl equivalent to 1% of the mass of the waste lubricating oil 2 , stirred for 5 minutes, and centrifuged to remove gum and asphalt. Add alkalized particles with a particle size of 60-100 mesh to the upper-stage filtrate through the alkalization degumming acid process at a liquid-solid volume ratio of 1:0.1, stir rapidly for 15 minutes, and then centrifugally filter. Add 50-100-mesh high-strength magnetic particles to the upper-stage filtrate at a liquid-solid volume ratio of 1:0.1 through the magnetic desquamation process, stir rapidly for 15 minutes, and centrifugally filter. Through carbon silica gel decolorization, the filtrate of the upper stage is filtered through a 1-10um activated carbon silica gel layer to obtain a purified oil containing...

Embodiment 3

[0031] Using tractor waste lubricating oil as raw material, heat the waste lubricating oil to 60°C through the dilution and degumming process, add n-heptane at a ratio of 1:1 to the volume of the oil agent, and then add CaCl equivalent to 3% of the mass of the waste lubricating oil 2 , stirred for 10 minutes, and centrifuged to remove gum and asphalt. Add alkalized particles with a particle size of 60-100 mesh to the upper-stage filtrate through the alkalization degumming acid process at a liquid-solid volume ratio of 1:0.2, stir rapidly for 10 minutes, and then centrifugally filter. Add 50-100-mesh high-strength magnetic particles to the upper-stage filtrate at a liquid-solid volume ratio of 1:0.2 through the magnetic desquamation process, stir rapidly for 10 minutes, and centrifugally filter. Through the carbon silica gel decolorization process, the upper-stage filtrate is filtered through a 1-10um activated carbon silica gel layer to obtain solvent-containing purified oil. ...

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Abstract

The present invention relates to a staged cleaning method for purifying waste lubricating oil, and the method mainly comprises the steps of diluting and degumming, alkalizing of a degumming acid, magnetic desorption for removing chips, carbon-silicon color filter and the like. Various impurities in the waste lubricating oil are removed by a chemical physical method, and problems that impurities such as asphalt and colloids are difficult to completely remove in an existing waste lubricating oil regeneration process are solved. By adopting the method of the invention, various impurities in the waste lubricating oil can be graded and removed to obtain high-quality purified oil, and the method has the advantages of simple operation, high impurity-removal efficiency and high quality of recovered oil.

Description

technical field [0001] The invention relates to the technical field of waste lubricating oil regeneration and utilization, in particular to a purification method for waste lubricating oil classification and impurity removal. Background technique [0002] After the lubricating oil in the locomotive has been operated and rubbed by the locomotive parts for a certain period of time, due to high-temperature oxidation, it gradually ages and deteriorates, and impurities such as asphalt, colloid, organic acid substances, metal impurities, and coke powder are produced by-products, forming waste lubricating oil. These impurities seriously affect the efficacy of the lubricating oil and must be removed. [0003] Chinese patent CN104498173A discloses a regeneration method for rubber-containing waste lubricating oil, which uses attapulgite concentrate adsorbent, high-alumina attapulgite concentrate adsorbent, siliceous sedimentary rock raw ore and siliceous volcanic acidic lava raw ore mi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M175/00
CPCC10M175/0016C10M175/0066C10M175/0083
Inventor 杨昌炎余洋张波吴金龙丁一刚
Owner 麻城天安化工股份有限公司