Compositions for topical application comprising benzoyl peroxide and adapalene
A technology of topical application of benzoyl peroxide, applied in the direction of active ingredients of peroxide compounds, medical preparations containing active ingredients, drug combinations, etc., can solve problems such as scaling and itching, ATRA instability, etc.
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[0101] According to one embodiment of the present invention, the method comprises:
[0102] (a) contacting the solid water-insoluble particulate material with a first cationic additive and an aqueous medium to obtain a dispersion of positively charged particulate material on its surface;
[0103] (b) subjecting the particulate material to a coating process comprising precipitating a metal oxide salt on the surface of the particulate material to form a metal oxide coating on the particulate material;
[0104] (b1) contacting the coated particulate material in an aqueous medium with a surface binding additive which is one or both of (i) a second cationic additive and (ii) a nonionic additive;
[0105] (b2) subjecting the granular material obtained in step (b1) to a coating process as in step (b);
[0106] (c) repeat steps (b1) and (b2) at least 3 times; and
[0107] (d) Aged metal oxide coating.
[0108] In addition, according to an embodiment of the present invention, the me...
Embodiment
[0161] In the following examples, all % values referring to solutions are (w / w).
[0162] All % values referring to dispersions (suspensions) are (w / w).
[0163] Unless otherwise stated, all solutions used in the following examples refer to aqueous solutions of the indicated components.
[0164] Example #1: Silica Encapsulation (Coating) of BPO
[0165] Step 1: Grinding: 110 g of 75% aqueous BPO (USP grade from Sigma, USA) was suspended in 152 g of 0.4% CTAC solution containing 0.001% silicon antifoam. BPO was ground using a rotor rotor mixer (IKA6100 operating at 15000 rpm). Grinding was stopped when the particle size distribution (PSD) of the suspension was d(0.9)≤35 μm or the temperature had reached 50°C. The final suspension was cooled to room temperature.
[0166] Step 2: Coating: During the coating process, the suspension was constantly stirred with a mechanical dissolver (60 mm, 500 RPM). The pH of the milled BPO suspension was corrected to 8 using NaOH 5...
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