A mussel shell coating with the function of purifying indoor air and its preparation method
A mussel shell and inner air technology, applied in the field of coatings, can solve problems such as low utilization rate of sunlight, unsatisfactory catalytic performance, and uneven quality
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Embodiment 1
[0028] Bi-Bi 2 o 3 / Preparation of micro-nano mussel shell composite materials: mussel shells are pre-treated, washed, air-dried, and calcined at 1000 degrees, then deeply damaged by a micro-nano pulverizer, and ground by a ball mill for 8 hours to prepare a micro-nano mussel shell material; the above materials are prepared according to the mass ratio 20:1 placed in 0.1mg / mL sodium dodecylsulfonate aqueous solution, stirred for 10h, centrifuged and dried to obtain micro-nano mussel shell modification materials; bismuth nitrate was added to ethanol solvent, stirred and mixed to obtain a concentration of 30mmol / L of bismuth nitrate solution; the micro-nano mussel shell modification material was added to the bismuth nitrate solution, mixed and stirred for 10 hours, and then placed in the reaction kettle, the filling degree of the reaction kettle was 90%, the heating rate was 2°C / min, and the temperature was 180°C. The reaction time is 10 hours, heating reaction; after the react...
Embodiment 2
[0031] Bi-Bi 2 o 3 / Preparation of micro-nano mussel shell composite materials: mussel shells are pre-treated, washed, air-dried, and calcined at 800 degrees, then deeply damaged by a micro-nano pulverizer, and ground by a ball mill for 10 hours to prepare a micro-nano mussel shell material; the above materials are prepared according to the mass ratio 50:1 in an aqueous solution of sodium dodecylsulfonate with a concentration of 1 mg / mL, stirred for 12 hours, and centrifuged to dry to obtain micro-nano mussel shell modification materials; add bismuth nitrate to ethanol solvent, stir and mix to obtain a concentration of 50 mmol / mL L of bismuth nitrate solution; add the micro-nano mussel shell modification material to the bismuth nitrate solution and mix and stir for 24 hours, then put it in the reaction kettle, the filling degree of the reaction kettle is 70%, the heating rate is 1°C / min, the temperature is 150°C, and the time is After heating for 36 hours, the reaction product...
Embodiment 3
[0034] Bi-Bi 2 o 3 / Preparation of micro-nano mussel shell composite materials: mussel shells are pre-treated, washed, air-dried, and calcined at 1200 degrees, then deeply damaged by a micro-nano pulverizer, and ground by a ball mill for 9 hours to prepare a micro-nano mussel shell material; the above materials are prepared according to the mass ratio 35:1 placed in 0.5mg / mL sodium dodecylsulfonate aqueous solution, stirred for 11h, centrifuged and dried to obtain micro-nano mussel shell modification materials; bismuth nitrate was added to ethanol solvent, stirred and mixed to obtain a concentration of 40mmol / L of bismuth nitrate solution; the micro-nano mussel shell modification material was added to the bismuth nitrate solution, mixed and stirred for 16 hours, and then placed in the reaction kettle, the filling degree of the reaction kettle was 80%, the heating rate was 1.5°C / min, and the temperature was 160°C. The reaction time is 24 hours, and the reaction is heated; aft...
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