Unlock instant, AI-driven research and patent intelligence for your innovation.
Non-metallic 1D/2D composite material, preparation method and application thereof
What is Al technical title?
Al technical title is built by PatSnap Al team. It summarizes the technical point description of the patent document.
A composite material and non-metallic technology, which is applied in the field of non-metallic 1D/2D composite materials and their preparation, can solve problems such as the impact of the photocatalytic performance of conductive polymer morphology, and achieve high photocatalytic water splitting hydrogen production performance, Excellent effect of photolysis of water and rich sources of raw materials
Active Publication Date: 2018-07-24
JIANGSU UNIV
View PDF2 Cites 1 Cited by
Summary
Abstract
Description
Claims
Application Information
AI Technical Summary
This helps you quickly interpret patents by identifying the three key elements:
Problems solved by technology
Method used
Benefits of technology
Problems solved by technology
But it has been reported and g-C 3 N 4 Only relatively simple conductive polymers such as polyaniline and polypyrrole are composited, and the reported literature does not mention the influence of the morphology and structure of the conductive polymer on the photocatalytic performance.
Method used
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more
Image
Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
Click on the blue label to locate the original text in one second.
Reading with bidirectional positioning of images and text.
Smart Image
Examples
Experimental program
Comparison scheme
Effect test
Embodiment 1
[0032] Embodiment 1: preparation g-C 3 N 4 catalyst of light
[0033] (1) Weigh urea, dry it in an oven at 80 °C for 24 h, grind it and put it into a crucible, cover it, and place it in a muffle furnace at 2.5 °C min -1 The heating rate was increased from room temperature to 550 °C and calcined for 4 h.
[0034] (2) Take it out and use 1 mol L -1 Pickle with nitric acid overnight, filter with suction, wash with distilled water 5-8 times until neutral, and dry overnight in a vacuum oven.
Embodiment 2
[0035] Example 2: Preparation of 1 wt% g-C 3 N 4 / PEDOT composite material
[0036] (1) Accurately weigh 0.9 g g-C 3 N 4 and 0.2 g FeCl 3 ·6H 2 O was dissolved in 50 mL deionized water, and then sonicated for 20 min.
[0037] (2) Then add 6.7 μL EDOT, and place the mixture in the reaction vessel.
[0038] (3) Finally, place the sealed reactor in an oven at 100 °C for 10 h.
[0039] (4) After the reaction, the reaction kettle was cooled to room temperature, and the product was suction filtered, washed and dried to obtain g-C 3 N 4 / PEDOT samples.
Embodiment 3
[0040] Embodiment 3: prepare 3 wt% g-C 3 N 4 / PEDOT composite material
[0041] (1) Accurately weigh 0.9 g g-C 3 N 4 and 0.2 g FeCl 3 ·6H 2 O was dissolved in 50 mL deionized water, and then sonicated for 20 min.
[0042] (2) Then add 20.1 μL EDOT, and place the mixture in the reaction vessel.
[0043] (3) Finally, place the sealed reactor in an oven at 100 °C for 10 h.
[0044] (4) After the reaction, the reaction kettle was cooled to room temperature, and the product was suction filtered, washed and dried to obtain g-C 3 N 4 / PEDOT samples.
[0045] Such as figure 1 is the g-C of this example 3 N 4 and g-C 3 N 4 The XRD spectrum of / PEDOT, after compounding,
[0046] g-C 3 N 4 The XRD diffraction peaks of PEDOT hardly changed, and the diffraction peaks of PEDOT and other substances were not observed, which may be because the content of PEDOT is too low relative to g-C3N4.
[0047] figure 2 For the pure g-C of this embodiment 3 N 4 and g-C 3 N 4 TEM ph...
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More
PUM
Login to View More
Abstract
The invention relates to a non-metallic 1D / 2D composite material, a preparation method and application thereof and belongs to the field of preparation of nano composite materials and clean energy. Thepreparation method comprises the following steps: firstly, preparing g-C3N4 for spare use; then preparing a g-C3N4 / PEDOT photocatalyst by adjusting the reaction conditions and the proportion of reactants. The PEDOT / g-C3N4 photocatalyst with a non-metallic 1D / 2D composite structure is prepared by utilizing a hydrothermal method and can be used for hydrogen production from photocatalytic decomposition of water under visible light; the obtained g-C3N4 / PEDOT sample has the 1D / 2D composite structure, the hydrogen producing amount can reach 3636.6mu mol g<-1> and is 5.5 times that of pure g-C3N4, therefore, the g-C3N4 / PEDOT composite photocatalyst with the 1D / 2D composite structure has large potential in the field of hydrogen production from photocatalytic decomposition of water.
Description
technical field [0001] The invention relates to a non-metallic 1D / 2D composite material and its preparation method and application, belonging to the field of preparation of nanocomposite materials and clean energy. Background technique [0002] With the continuous development of human society, the demand for energy continues to expand, which has led to the burning of a large amount of fossil fuels and caused serious harm to the ecological environment. However, traditional fossil fuels will also be exhausted in the near future, which may cause even more severe energy shortages. As a clean energy, hydrogen has the advantages of abundant raw materials, cheap, non-toxic and harmless, and high production capacity compared with traditional energy sources. However, hydrogen naturally exists on the earth in very small amounts. Therefore, the use of semiconductors to catalyze the photolysis of water to produce hydrogen has attracted extensive attention from scientific researchers. ...
Claims
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More
Application Information
Patent Timeline
Application Date:The date an application was filed.
Publication Date:The date a patent or application was officially published.
First Publication Date:The earliest publication date of a patent with the same application number.
Issue Date:Publication date of the patent grant document.
PCT Entry Date:The Entry date of PCT National Phase.
Estimated Expiry Date:The statutory expiry date of a patent right according to the Patent Law, and it is the longest term of protection that the patent right can achieve without the termination of the patent right due to other reasons(Term extension factor has been taken into account ).
Invalid Date:Actual expiry date is based on effective date or publication date of legal transaction data of invalid patent.
Login to View More 
Login to View More