A kind of preparation method of high-purity oxygen-free high silver-containing copper rod
A high-purity, copper rod technology is applied in the field of preparation of high-purity, oxygen-free and high-silver-containing copper rods, which can solve the problems of increasing product contact resistance, low yield, shortening material service life, etc., and achieves increased tensile strength and extension. rate, improved anti-oxidative properties, and good anti-oxidative properties
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Embodiment 1
[0024] A method for preparing a high-purity oxygen-free high silver-containing copper rod is prepared by an up-drawing process, comprising the following steps:
[0025] (1) Ingredients: Prepare the raw materials in the following weight percentages: 0.009% silver, 0.018% zirconium, 0.015% chromium, and 99.958% copper, wherein silver is selected from silver ingots with a purity of 99.99%, and the resistivity of silver at 20° C. is 1.784 μΩ. cm, the copper is high-purity cathode electrolytic copper;
[0026] (2) Place the high-purity cathode electrolytic copper to be used above the uplink power frequency furnace for baking, and bake out the moisture in the electrolytic copper;
[0027] (3) Melting the raw materials in step (1) into a solution at 1288°C, adding other raw materials in step (1) for each row of electrolytic copper, so that the weight percentage of each raw material meets the requirements;
[0028] (4) In the melting step (1) raw materials are covered with graphite f...
Embodiment 2
[0032] A method for preparing a high-purity oxygen-free high silver-containing copper rod is prepared by an up-drawing process, comprising the following steps:
[0033] (1) Ingredients: Prepare the raw materials in the following weight percentages: 0.03% silver, 0.03% zirconium, 0.022% chromium, and 99.918% copper, wherein silver is selected from silver ingots with a purity of 99.99%, and the resistivity of silver at 20° C. is 1.821 μΩ. cm, the copper is high-purity cathode electrolytic copper;
[0034] (2) Place the high-purity cathode electrolytic copper to be used above the uplink power frequency furnace for baking, and bake out the moisture in the electrolytic copper;
[0035] (3) Melting the raw materials in step (1) into a solution at 1350°C, adding other raw materials in step (1) for each row of electrolytic copper, so that the weight percentage of each raw material meets the requirements;
[0036] (4) In the melting step (1) raw materials are covered with graphite fla...
Embodiment 3
[0040] A method for preparing a high-purity oxygen-free high silver-containing copper rod is prepared by an up-drawing process, comprising the following steps:
[0041](1) Ingredients: Prepare the raw materials in the following weight percentages: 0.18% silver, 0.045% zirconium, 0.029% chromium, and 99.746% copper, wherein silver is selected from silver ingots with a purity of 99.99%, and the resistivity of silver at 20° C. is 1.848 μΩ. cm, the copper is high-purity cathode electrolytic copper;
[0042] (2) Place the high-purity cathode electrolytic copper to be used above the uplink power frequency furnace for baking, and bake out the moisture in the electrolytic copper;
[0043] (3) Melting the raw materials in step (1) into a solution at 1460° C., adding other raw materials in step (1) for each row of electrolytic copper, so that the weight percentage of each raw material meets the requirements;
[0044] (4) In the melting step (1) raw materials are covered with graphite f...
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Abstract
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