Hand washing solution and preparation method thereof
A technology of hand sanitizer and raw materials, applied in the field of daily chemicals, can solve the problems of poor sterilization effect and obvious bacteriostatic effect, and achieve the effect of significant killing and inhibition effect, obvious effect and simple formula.
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Embodiment 1
[0045] The preparation of embodiment 1 hemp extract
[0046] (1) Wash and air-dry the raw material cannabis stalks, cannabis flowers, cannabis leaves and / or cannabis roots;
[0047] (2) pulverize the above-mentioned air-dried raw materials to 10-40 mesh;
[0048] (3) Extract the obtained powder by cold soaking with 4-8 times the amount of 30%-60% ethanol for 1-3 times, each time for 0.5-2 hours;
[0049] (4) Combine the extracts and decolorize through 0.1-1wt% activated carbon adsorption;
[0050] (5) Concentrate under reduced pressure to a relative density of 1.01-1.03 at a temperature of 70°C;
[0051] Cannabis extract extracts are obtained, such as cannabis stalk core extract, cannabis flower extract, cannabis leaf extract, or a combination of two or three of them.
Embodiment 2
[0052] The preparation of embodiment 2 hemp extract
[0053] (1) using about 8-10 times the weight of the extraction solvent or its mixture to heat and reflux the stalk core, flowers, leaves and / or roots of cannabis for at least 1 hour;
[0054] (2) remove residue by filtration, and remove solvent under vacuum condition;
[0055] (3) heating the obtained extract at a temperature of about 110-135° C. for about 40 minutes;
[0056] (4) followed by chromatographic separation.
[0057] Described extraction solvent can be low-molecular-weight alcohol (such as methanol, ethanol, butanol or propanol); Acetate (such as methyl acetate or ethyl acetate); Ketone (such as acetone); Ether (such as methyl ether or ether) ; Low boiling aliphatic or aromatic hydrocarbons or chlorinated hydrocarbons.
[0058] In the chromatographic separation, the mobile phase mixture used in the chromatography is composed of methanol / water and acetic acid or ethanol / water and acetic acid.
Embodiment 3
[0059] The preparation of embodiment 3 hemp extract
[0060] (1) Using about 3-10 times the weight of the extraction solvent or its mixture to heat and reflux the stalk core, flowers, leaves and / or roots of cannabis for at least 1 hour;
[0061] (2) filter to remove residue;
[0062] (3) extracting at least twice with 1%-10% aqueous sodium hydroxide solution containing about 20wt% ethanol;
[0063] (4) The extract is mixed with 5% sulfuric acid solution so that the pH value is about 2-4;
[0064] (5) Then use a low-boiling point solvent (such as low-boiling point aliphatic hydrocarbons, aromatic hydrocarbons, chlorinated hydrocarbons, methyl acetate, ethyl acetate or mixtures thereof) to extract at least twice, and remove the solvent under low-temperature vacuum;
[0065] (6) followed by chromatographic separation.
[0066] Described extraction solvent can be low-molecular-weight alcohol (such as methanol, ethanol, butanol or propanol); Acetate (such as methyl acetate or et...
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