Adhesive sheet for conductive members, conductive member laminate and image display device
A technology for conductive members and adhesive sheets, applied in the field of conductive member laminates and adhesive sheets for conductive members, can solve problems such as oxidation and deterioration of adherends, and achieve good curing properties, foaming resistance, and reliable curing properties.
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Embodiment 1
[0166] Add propoxylate as a crosslinking agent to 1 kg of a copolymer (A-1, mass average molecular weight: 400,000) formed by 76 parts by mass of 2-ethylhexyl acrylate, 20 parts by mass of vinyl acetate, and 4 parts by mass of acrylic acid. 200 g of alkylated pentaerythritol polyacrylate (manufactured by Shin-Nakamura Chemical Industry Co., Ltd., trade name "ATM-4PL"), and 4-methylbenzophenone and 2,4,6-trimethyl 10 g of a mixture of benzophenone (manufactured by Lamberti, trade name "Esacure TZT") was uniformly mixed to obtain a resin composition for an intermediate layer.
[0167] Two sheets of polyethylene terephthalate films (manufactured by Mitsubishi Plastics, Inc., trade name "Diafoil MRF", thickness 75 µm, and Mitsubishi Plastics, Inc., trade name "Diafoil MRT", thickness 38 μm) sandwiched the resin composition for an intermediate layer, and shaped into a sheet shape so that the thickness of the adhesive sheet became 80 μm, to prepare a resin sheet for an intermediate ...
Embodiment 2
[0174] Add 1,2 , 3 g of 3-triazole, 3 g of tridecyl phosphite (manufactured by ADEKA Corporation, trade name “ADK STAB 3010”) as a phosphite compound, pentaerythritol triacrylate and pentaerythritol tetraacrylate (East Asia Synthesize 20 g of "ARONIX M-306", manufactured by Co., Ltd., and 10 g of 1-hydroxy-cyclohexyl phenyl ketone (Irgacure 184, manufactured by BASF Corporation) as a photopolymerization initiator, and mix them uniformly to obtain a resin for an adhesive layer combination.
[0175] Next, the resin composition for the pressure-sensitive adhesive layer was formed on a polyethylene terephthalate film (manufactured by Mitsubishi Plastics, Inc., Diafoil MRV, thickness 100 μm) that had undergone release treatment so as to have a thickness of 150 μm. After the sheet was formed, it was covered with a peeled polyethylene terephthalate film (manufactured by Mitsubishi Plastics, Inc., trade name "Diafoil MRQ", thickness 75 µm). The cumulative light intensity at a wavele...
Embodiment 3
[0177] As the phosphite compound, 3,9-bis(decyloxy)-2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane (Johoku Chemical Co., Ltd. manufactured, trade name "JPE-10") 3g, it carried out similarly to Example 2, and produced the adhesive sheet laminated body 3. The following various evaluations were performed on the pressure-sensitive adhesive sheet laminate 3 . The results are shown in Table 1.
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