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A kind of preparation method of geotechnical composite anti-seepage material

A compound anti-seepage and kneader technology, which is applied in the field of preparation of geotechnical composite anti-seepage materials, can solve the problems of loss of anti-seepage effect, uncoordinated deformation, fracture, etc., to achieve improved compatibility, low cost, and avoid excessive pores big effect

Active Publication Date: 2019-09-13
高松
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the common geotechnical composite anti-seepage materials currently on the market are prone to deformation and incongruity under complex hydraulic loads, and then appear to break, losing the anti-seepage effect

Method used

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  • A kind of preparation method of geotechnical composite anti-seepage material

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Embodiment 1

[0016] A preparation method of a geotechnical composite anti-seepage material, comprising the following steps:

[0017] (1) In parts by weight, mix 36 parts of EPDM rubber powder and 55 parts of polyethylene masterbatch evenly, then add them to 70 parts of modified liquid, heat the mixture to 88°C, and heat it for 2 hours. Then filter, and add the filter residue to a kneader for mixing to obtain a copolymer, wherein the modified liquid is made of the following components by weight: 6 parts of isopropanol pinacol borate, 3 parts of D-methyl lactate 11 parts of castor oil, 39 parts of absolute ethanol;

[0018] (2) In parts by weight, add 46 parts of copolymer, 2 parts of coupling agent, 4 parts of triethyl trimesate, and 5 parts of tetrabutylammonium fluoride into the extruder, and extrude for 2 minutes;

[0019] (3) Add the salt solution dropwise into the plasticizing section of the extruder, and then extrude, cool, and granulate to obtain a functional masterbatch, wherein th...

Embodiment 2

[0024] A preparation method of a geotechnical composite anti-seepage material, comprising the following steps:

[0025] (1) In parts by weight, mix 38 parts of EPDM rubber powder and 58 parts of polyethylene masterbatch evenly, add them to 73 parts of modified liquid, heat the mixture to 90°C, and heat it for 2.5 hours. Then filter, and add the filter residue to a kneader for mixing to obtain a copolymer, wherein the modified liquid is made of the following components by weight: 7 parts of isopropanol pinacol borate, 4 parts of D-methyl lactate 13 parts of castor oil, 41 parts of absolute ethanol;

[0026] (2) In parts by weight, add 50 parts of copolymer, 3 parts of coupling agent, 6 parts of triethyl trimesate, and 7 parts of tetrabutylammonium fluoride into the extruder, and extrude for 3 minutes;

[0027] (3) Add the salt solution dropwise into the plasticizing section of the extruder, and then extrude, cool, and granulate to obtain a functional masterbatch, wherein the s...

Embodiment 3

[0032] A preparation method of a geotechnical composite anti-seepage material, comprising the following steps:

[0033] (1) In parts by weight, mix 42 parts of EPDM rubber powder and 60 parts of polyethylene masterbatch evenly, add them to 75 parts of modified liquid, heat the mixture to 92 ° C, and heat-preserve it for 3 hours. Then filter, add the filter residue to a kneader and knead to obtain a copolymer, wherein the modified liquid is made of the following components by weight: 8 parts of isopropanol pinacol borate, 5 parts of D-methyl lactate 14 parts of castor oil, 44 parts of absolute ethanol;

[0034] (2) In parts by weight, add 52 parts of copolymer, 5 parts of coupling agent, 8 parts of triethyl trimesate, and 9 parts of tetrabutylammonium fluoride into the extruder, and extrude for 4 minutes;

[0035] (3) Add the salt solution dropwise into the plasticizing section of the extruder, and then extrude, cool, and granulate to obtain a functional masterbatch, wherein t...

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Abstract

The invention discloses a preparation method of a geotechnical composite anti-seepage material. The preparation method includes the steps of firstly, evenly mixing ethylene propylene diene monomer powder and polyethylene master batch, adding into modification liquid, heating the mixture, performing heat preservation, filtering, and adding the filter residues into a kneading machine for mixing to obtain copolymer; secondly, adding the copolymer, a coupling agent, triethyl benzenetricarboxylate and tetrabutyl ammonium fluoride into an extruding machine, and performing extruding reaction for 2-4minutes; thirdly, dropwise adding a salt solution into an extruder plasticizing section, and performing extrusion, cooling and granulation to obtain functional master batch; fourthly, performing rolling compositing, cooling and slicing on the functional master batch obtained in the third step to prepare the geotechnical composite anti-seepage material. The prepared geotechnical composite anti-seepage material is excellent in corrosion resistance, oxidation resistance, water resistance and mechanical performance and cannot break under hydraulic load.

Description

technical field [0001] The invention belongs to the technical field of preparation of anti-seepage materials for water conservancy projects, and in particular relates to a preparation method of geotechnical composite anti-seepage materials. Background technique [0002] Geotechnical composite anti-seepage material is a kind of flat geotechnical composite material prepared by compounding relatively impermeable polymer synthetic materials (including natural materials) and geotextiles through a certain process. Geotechnical composite anti-seepage material is an important part of the dam (reservoir) anti-seepage system. The direct exposure of geotechnical composite anti-seepage material is superior to other methods in terms of engineering construction, cost, and benefit. It is the future dam anti-seepage The main development trend of the structure. However, the common geotechnical composite anti-seepage materials currently available on the market are prone to deformation and un...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L23/06C08L23/16C08L91/00C08L35/00C08K5/12C08K5/19C08K3/24C08K5/10C08K13/02
Inventor 高松
Owner 高松