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Partition agent for ferrite body and its preparation and treatment method after use

A technology of release agent and ferrite, which is applied in chemical instruments and methods, oxidized water/sewage treatment, water/sewage treatment, etc., can solve the problems of kerosene volatilization, great harm to human body, manual wiping, etc., and achieve cost reduction, Good demoulding effect and good stability

Active Publication Date: 2021-09-24
ZHEJIANG NANCI IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In the prior art, saponification fluid, cutting fluid, engine oil (lubricating oil, kerosene, diesel oil, etc.) are used as release agents in the processing of magnetic material blanks. The existing disadvantages are: raw materials are not environmentally friendly, easy to stick to molds during molding, manual wiping is required, waste water The content of phosphorus and ammonia nitrogen in medium is high; some large-scale enterprises, in order to improve production efficiency and ensure product quality, mix the release agent with diesel or kerosene. The aromatic content of diesel is relatively high, which is relatively harmful to the human body. Containing aromatic hydrocarbons, nitrogen, oxygen, sulfur, etc. are also relatively harmful to the human body
The use of diesel or kerosene in the release agent will undoubtedly increase the production cost, not only increase the difficulty of workers' operation, but also the diesel or kerosene in the wastewater will increase the difficulty of wastewater treatment, poor biodegradability, and greatly increase the COD in wastewater
For example, the patent application publication number CN 1843655A discloses a wet-forming release agent for magnetic materials and its preparation method. The release agent uses kerosene as a medium, which increases the difficulty of wastewater treatment; patent announcement number: CN 102085563 A, which discloses A release agent and a preparation method thereof, the release agent contains a gasoline mixture with a weight percentage of 88-99.5%, which also increases the difficulty of wastewater treatment

Method used

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  • Partition agent for ferrite body and its preparation and treatment method after use

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A release agent for ferrite body, the release agent is composed of base oil, emulsifier, anti-rust agent, the parts by weight of each component are: 45 parts of base oil, 45 parts of emulsifier, 10 parts of anti-rust agent ; Described base oil is the mixture of 15 parts by weight of Fuchs oil and 30 parts by weight of propylene oxide condensate; Described emulsifier is 35 parts by weight of fatty alcohol polyoxyethylene ether and parts by weight A mixture of 10 parts of sorbitan fatty acid ester; the antirust agent is a mixture of 4 parts by weight of triethanolamine oleic acid soap and 6 parts by weight of oleic acid diethanolamide; the above-mentioned release agent can be diluted into release agent by distilled water For the diluent, the ratio of parts by weight of the release agent to distilled water is 1:20.

Embodiment 2

[0033] A method for preparing a release agent for a ferrite body, first mixing 35 parts by weight of fatty alcohol polyoxyethylene ether and 10 parts by weight of sorbitan fatty acid ester to make an emulsifier; 15 parts of Fox oil and 30 parts by weight of propylene oxide condensate are mixed to obtain base oil; 4 parts by weight of triethanolamine oleic acid soap and 6 parts by weight of oleic acid diethanolamide are mixed to obtain anti rust agent; slowly add the base oil prepared above in the emulsifier prepared above, and carry out the dropwise addition at a temperature of 30 ° C, a stirring speed of 500 rpm, and mixing and stirring for 30 minutes; then add the anti-rust agent prepared above agent, continue to stir for 30 minutes, that is, it is prepared as a release agent for ferrite body. Dilute the release agent with distilled water at a ratio of 1:20 to form a release agent diluent before use. The water spray speed during dilution is 400mm / s, and the water spray time ...

Embodiment 3

[0035]A treatment method for the use of the release agent for ferrite blanks. The waste liquid formed after the use of the release agent is continuously processed under the conditions of temperature 180°C, pressure 2Mpa, and rotation speed 600r / min by using a kettle-type reaction process. After reacting for 2 hours, catalytic oxidation treatment was carried out on the waste liquid of the separator; after the treatment, it became clear and transparent, the content of ammonia nitrogen increased by 30%, the content of total phosphorus decreased by 70%, and the removal rate of COD could reach 76.6%.

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Abstract

The invention relates to a release agent for a ferrite blank, its preparation and its post-use treatment method, which belong to the technical field of magnetic material blank forming processing aids. It is characterized in that: the release agent is composed of base oil, emulsifier, and antirust agent, and the parts by weight of each component are: 15-50 parts of base oil, 20-60 parts of emulsifier, and 5-10 parts of antirust agent; The base oil is any one or more of 5# white oil, 7# white oil, 10# white oil, Foss oil or propylene oxide condensate. The invention can meet the production process requirements of the ferrite body, and has a good demoulding effect; the synthetic raw material of the release agent is green and environmentally friendly, non-toxic and harmless, greatly reduces the content of phosphorus and ammonia nitrogen in the release agent wastewater, and overcomes the COD High disadvantages, avoiding excessive discharge of pollutants; the release agent and the release agent diluted with distilled water have good stability, and the waste water generated after the release agent is released from the mold is easy to handle and can be recycled.

Description

technical field [0001] The invention relates to a release agent for a ferrite green body, its preparation and a treatment method after use, and belongs to the technical field of magnetic material green body forming and processing aids. Background technique [0002] There are many magnetic material enterprises in the world, and there are many in our country, especially in Zhejiang Province, which has the industrial advantages of magnetic materials. Ferrite is a new type of non-metallic magnetic material developed in the 1940s. Ferrite generally refers to the composite oxide of iron group and one or more other metal elements. It belongs to semiconductor. It is used as Magnetic media are used. [0003] The production process of ferrite body magnets: mixing ferric oxide + barium carbonate or strontium carbonate in proportion → green body pressing → sinteringgrinding and milling to make raw material powderraw material powder + water + other ingredients in proportion by wei...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M173/00C10M175/00C02F1/72C10N40/36
CPCC02F1/725C10M173/00C10M175/00C10M2203/1006C10M2207/289C10M2209/104C10M2209/1055C10M2209/108C10M2215/082C10N2040/36C10N2030/64
Inventor 苟明霞陈革新赵培庆
Owner ZHEJIANG NANCI IND CO LTD
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