Preparation method of toughened pressure-resistant ablation-resistant material
An ablation-resistant and toughening technology, applied in chemical instruments and methods, lamination, lamination devices, etc., can solve the problems of poor high-temperature compression resistance, high brittleness of phenolic resin, high molding shrinkage and difficult processing, etc. The effect of improving thermal insulation performance, large thermal conductivity, and increasing heat dissipation area
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[0023] Take 150~200mL of methyl silicone oil into a three-necked flask with a thermometer and a reflux device, move the three-necked flask into a sand bath under the protection of nitrogen, control the temperature of the sand bath to 420~430℃, keep it warm for 1~2h after reaction To 460~480℃, continue to keep the temperature and react for 40~50min. After the reaction, cool to room temperature naturally to obtain the product; add 200~300mL xylene to the above product, stir and mix for 10~15min, then filter to obtain the filtrate, and transfer the filtrate to In a rotary evaporator, rotate and concentrate at 80~90℃ for 40~50min to obtain a concentrated solution. Take 30~40g of zirconium boride and add it to the pulverizer to pulverize for 30~40min to obtain zirconium boride powder. , Concentrated solution, 100~200mL deionized water were added to the beaker, stirred and mixed for 15~20min to obtain the binding agent; in parts by weight, 40~50 parts of white corundum, 30~40 parts of...
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