Multifunctional air purificant and preparation method
An air purifier and multi-functional technology, applied in the field of air purification, can solve the problems of bamboo vinegar liquid's volatile antibacterial activity, unstable antibacterial activity, single purification function, etc., achieve high utilization rate of visible light, excellent antibacterial effect, The effect of high degradation efficiency
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Embodiment 1
[0031] (1) Add activated carbon granules to the stock solution of bamboo vinegar, stir for 48 minutes at room temperature, filter with suction, then place the filtrate in a distillation apparatus, heat it in a water bath under vacuum conditions, remove low boiling point components, and obtain refined bamboo vinegar solution; The heating temperature is 56° C., the vacuum degree is 0.05 MPa, and the time is 70 minutes; the parts by weight of each raw material are 28 parts by weight of activated carbon particles, and 72 parts by weight of bamboo vinegar stock solution;
[0032] (2) Add macroporous polystyrene-divinylbenzene adsorption resin to tetrahydrofuran for swelling, then add anhydrous aluminum trichloride, heat to reflux for 9 hours, further add trimellitic anhydride to reflux for 17 hours, and then wash with methanol for 4 hours Once, vacuum-dried to obtain the macroporous polystyrene-divinylbenzene adsorption resin of chloromethylation modified by acid groups; the heating...
Embodiment 2
[0036] (1) Add activated carbon granules to the stock solution of bamboo vinegar, stir at room temperature for 45 minutes, filter with suction, then place the filtrate in a distillation apparatus, and heat it in a water bath under vacuum conditions to remove low-boiling components to obtain refined bamboo vinegar; The heating temperature is 52° C., the vacuum degree is 0.04 MPa, and the heating time is 80 minutes; the parts by weight of each raw material are 25 parts by weight of activated carbon particles, and 75 parts by weight of bamboo vinegar stock solution;
[0037] (2) Add macroporous polystyrene-divinylbenzene adsorption resin to tetrahydrofuran for swelling, then add anhydrous aluminum trichloride, heat to reflux for 8.5 hours, further add trimellitic anhydride to reflux for 19 hours, and then wash with methanol 3 times, vacuum-dried to obtain the chloromethylated macroporous polystyrene-divinylbenzene adsorption resin modified by acidic groups; the heating temperature...
Embodiment 3
[0041] (1) Add activated carbon granules to the stock solution of bamboo vinegar, stir at room temperature for 55 minutes, filter with suction, then place the filtrate in a distillation apparatus, and heat it in a water bath under vacuum conditions to remove low-boiling components to obtain refined bamboo vinegar; The heating temperature is 58° C., the vacuum degree is 0.07 MPa, and the heating time is 70 minutes; the parts by weight of each raw material are 35 parts by weight of activated carbon particles and 65 parts by weight of bamboo vinegar stock solution;
[0042] (2) Add macroporous polystyrene-divinylbenzene adsorption resin to tetrahydrofuran for swelling, then add anhydrous aluminum trichloride, heat to reflux for 9.5 hours, further add trimellitic anhydride to reflux for 16 hours, and then wash with methanol 5 times, vacuum-dried to obtain the chloromethylated macroporous polystyrene-divinylbenzene adsorption resin modified by acidic groups; the heating temperature ...
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