A magnesium alloy with high medical performance
A magnesium alloy and performance technology, applied in the field of selective laser melting preparation process and heat treatment, can solve the problems of loss of mechanical integrity, corrosion resistance, poor wear resistance, etc., and achieve excellent mechanical compatibility and excellent biocompatibility. Effect
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Embodiment 1
[0034] 1. Composition of the above alloy powder: 2% molybdenum; 1% tantalum; 0.5% chromium; 5% titanium; the rest is composed of magnesium and inevitable impurities such as C, S, and P. Pour the above powder into the miniature omnidirectional planetary ball mill F-P400E, and the rotation speed of the ball mill tank is 600r / min, so that the metal powder is fully mixed and ground.
[0035] 2. If figure 1 As shown, the selective laser ablation method
[0036] Use SLM Solutions 500 to process the mixed powder after ball milling obtained in step (1); SLM parameters include laser power of 110W, fiber laser spot size of 0.15mm, groove spacing of 0.10mm, powder layer thickness of 0.03mm; using 200mm / s scanning speed to prepare a cylindrical sample with a size of 10mm×5mm. The temperature rise rate in the SLM system is 10°C / s, input protective gas nitrogen, the concentration of nitrogen is 1800cc, rise to the preset temperature of 1200°C, keep warm for 4 hours, the protective gas is...
Embodiment 2
[0040] 1. Composition of the above alloy powder: 3% molybdenum; 2% tantalum; 1.5% chromium; 10% titanium; the rest is composed of magnesium and inevitable impurities such as C, S, and P. Pour the above powder into the miniature omni-directional planetary ball mill F-P400E, and the ball milling tank rotates at 700r / min to fully mix and grind the metal powder.
[0041] 2. If figure 1 As shown, the selective laser ablation method
[0042]SLM Solutions 500 was used to process the ball-milled mixed powder obtained in step (1); SLM parameters included laser power of 115W, spot size of 0.18mm, groove spacing of 0.11mm, and powder layer thickness of 00.4mm. Cylindrical samples with a size of 10 mm×5 mm were prepared at a scanning speed of 220 mm / s. The temperature rise rate in the SLM system is 15°C / s, input protective gas nitrogen, the concentration of nitrogen is 1800cc, rise to the preset temperature of 1300°C, and keep warm for 4.5 hours: the protective gas is: nitrogen for 1 ho...
Embodiment 3
[0046] 1. Composition of the above alloy powder: 4.5% molybdenum; 3% tantalum; 2.5% chromium; 10% titanium; the rest is composed of magnesium and inevitable impurities such as C, S, and P. Pour the above powder into the miniature omnidirectional planetary ball mill F-P400E, and the rotation speed of the ball mill tank is 750r / min, so that the metal powder is fully mixed and ground.
[0047] 2. If figure 1 As shown, the selective laser ablation method
[0048] Use SLM Solutions 500 to process the mixed powder after ball milling obtained in step (1); SLM parameters include laser power of 125W, spot size of 0.18mm, groove spacing of 0.11mm, and powder layer thickness of 0.06mm; using 250mm / s A cylindrical sample with a size of 10 mm × 5 mm was prepared at a scanning speed of 10 mm. The temperature rise rate in the SLM system is 35°C / s, input protective gas nitrogen, the concentration of nitrogen is 1800cc, rise to the preset temperature of 1450°C, and keep warm for 6 hours, in ...
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