Active ray-sensitive or radiation-sensitive resin composition, pattern formation method, and electronic device production method
A technology of sensitizing rays and resin composition, which is applied in the photoplate-making process of the patterned surface, photosensitive material processing, instruments, etc., can solve the problems of damage to the exposure machine and difficulty in simultaneously satisfying the problem, and achieve excellent degassing performance and exposure tolerance Excellent effect
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[0508] Hereinafter, the present invention will be described in further detail through examples, but the present invention is not limited thereto.
[0509]
Synthetic example 1
[0510] Synthesis Example 1: Synthesis of Resin (A-19)
[0511]4.9 g of monomer (1), 6.7 g of monomer (2), 9.1 g of monomer (3) and 0.50 g of polymerization initiator V-601 (manufactured by Wako Pure Chemical Industries, Ltd.) were dissolved in 76.1 g of cyclohexanone. 41.0 g of cyclohexanone was put into the reaction container, and it was dripped in the system of 85 degreeC over 4 hours under nitrogen atmosphere. After the reaction solution was heated and stirred for 2 hours, it was cooled to room temperature. The reaction solution was added dropwise to 1377 g of a mixed solution of n-heptane and ethyl acetate (n-heptane / ethyl acetate=9 / 1 (mass ratio)) to precipitate a polymer, followed by filtration. The filtered solid was washed with 413 g of a mixed solution of n-heptane and ethyl acetate (n-heptane / ethyl acetate=9 / 1 (mass ratio)). Then, the washed solid was dried under reduced pressure to obtain 12.4 g of resin (A-19). The weight average molecular weight obtained by GP...
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