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A magnetic recording material and a preparation method thereof

A magnetic recording and oxide technology, applied in magnetic recording, data recording, recording information storage, etc., can solve the problems of coercivity, remanence, and steep hysteresis loop performance, etc., to avoid coercivity The effect of excessive force, fine particle size, and improvement of uniform dispersion

Active Publication Date: 2019-05-10
BGRIMM TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The first object of the present invention is to provide a magnetic recording material to solve the technical problems in the prior art that cannot take into account coercive force, remanence, steep hysteresis loop and other performances

Method used

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  • A magnetic recording material and a preparation method thereof

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preparation example Construction

[0052] The present invention also provides a method for preparing the magnetic recording material, comprising the steps of:

[0053] The raw materials are mixed in proportion, densified, pelletized, pre-fired at 1050-1200° C. for 1-4 hours, coarsely crushed and then finely ground, and tempered at 960-1020° C. for 1-4 hours to obtain the magnetic recording material.

[0054] In a preferred embodiment of the present invention, after pre-burning at 1050-1100°C for 1-2 hours, the temperature is raised to 1150-1200°C for 1-2 hours.

[0055] In a preferred embodiment of the present invention, the densification treatment includes: using an ore mill for densification treatment for 30-90s.

[0056] In a preferred embodiment of the present invention, the size of the pelletized pellets is 50-500 μm.

[0057] In a preferred embodiment of the present invention, after pre-calcination, it is coarsely crushed to a particle size of 2.0-2.2 μm.

[0058] In a preferred embodiment of the presen...

Embodiment 1

[0061] The preparation method of the magnetic recording material described in the present embodiment, the steps are as follows:

[0062] (1) In parts by weight, weigh 135 parts of iron red (Tangshan Iron and Steel Group), 25 parts of strontium carbonate, 30 parts of barium carbonate, 1.2 parts of samarium oxide, 1.2 parts of titanium oxide, 1.6 parts of cobalt oxide, and 1.6 parts of zirconium oxide , 1.6 parts of nickel oxide, and 2 parts of bismuth trioxide, mixed and placed in an ore mill, after densification treatment for 60 seconds, pelletized with water, the size of the pellets is 200 μm;

[0063] (2) The pellets obtained in step (1) were pre-calcined at 1080°C for 2 hours, and after the pre-calcination was completed, they were coarsely crushed with a ball mill until the average particle size was 2.0 μm;

[0064] (3) placing the coarsely crushed material obtained in step (2) in a ball mill, and finely grinding it until the average particle size is 1.5 μm;

[0065] (4) T...

Embodiment 2

[0067] The present embodiment refers to the preparation method of Example 1, and the only difference is that the raw materials of this embodiment are 120 parts by weight of iron red (Tangshan Iron and Steel Group), 12 parts of strontium carbonate, 28 parts of barium carbonate, and 1 part of samarium oxide. 0.9 parts of titanium oxide, 1.7 parts of cobalt oxide, 1.7 parts of zirconium oxide, 1.7 parts of nickel oxide, and 1 part of bismuth trioxide.

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Abstract

The invention relates to the technical field of magnetic materials, in particular to a magnetic recording material and a preparation method thereof. The magnetic recording material is mainly preparedfrom the following components in parts by weight: 100-100 parts of iron oxide, 15-30 parts of strontium salt, 25-35 parts of barium salt, 0.5-2 parts of samarium oxide, 4-10 parts of additive and 1-3parts of flux; wherein the additive comprises one or more of oxides of titanium, oxides of cobalt, oxides of zirconium and oxides of nickel. The magnetic recording material provided by the invention can give consideration to coercive force, residual magnetism and steep hysteresis loop; Any one or more additives of Ti, Co, Zr and Ni are added, so that the coercive force is maximized as much as possible within a reasonable range, a lower SFD value is obtained, and the magnetic recording material has a steep hysteresis loop; and various additives partially serve as dispersion phases to hinder grain boundary movement, refine the particle size of the magnetic material and improve the uniform dispersity.

Description

technical field [0001] The invention relates to the technical field of magnetic materials, in particular to a magnetic recording material and a preparation method thereof. Background technique [0002] With the rapid development of science and technology, magnetic recording materials have been widely used in the storage of electronic data. As a magnetic recording material, the main requirements include high coercive force, appropriately high saturation magnetization, high remanence ratio, steep hysteresis loop, low magnetic temperature coefficient and aging coefficient, etc. High coercive force can improve the density and anti-interference of stored information, appropriately high saturation magnetization can increase the output information intensity, high remanence ratio can improve information recording efficiency and reduce self-demagnetization effect, steep hysteresis The loop can improve the resolution of the recorded information, and the low magnetic temperature coeff...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G11B5/65G11B5/84
Inventor 刘荣明张威峰刘辉王常蕾王继全王倩贾立颖李炳山
Owner BGRIMM TECH CO LTD