Preparing method of low-allergenicity ovalbumin peptide
A low-sensitivity technology for ovalbumin, applied in the field of preparation of low-sensitivity ovalbumin peptides, can solve the problems of reducing molecular weight and reducing allergenicity
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Embodiment 1
[0019] A method for preparing a low-sensitivity ovalbumin peptide, comprising the steps of:
[0020] (1) Pretreatment: prepare food-grade hydrogen peroxide with a mass fraction of solute of 0.1%, according to the mass ratio ovalbumin: food-grade hydrogen peroxide: potassium citrate: calcium chloride = 10:0.1:0.06:0.01, the Add high-grade hydrogen peroxide into the ovalbumin, fully stir and mix, then add potassium citrate and calcium chloride to the mixture in turn to obtain mixture A;
[0021] (2) Glycosylation: Dissolve 30 parts of mixed material A and 30 parts of glucose in deionized water in parts by mass, and mix evenly after dissolving. The quality of deionized water is 5 times the total mass of mixed material A and glucose to be dissolved ; After mixing evenly, freeze-drying, and after freeze-drying, react for 1 hour at a relative humidity of 60% to 80% and a temperature of 50 to 70°C to obtain sample B;
[0022] (3) Enzymolysis: add pepsin enzymolysis solution whose ma...
Embodiment 2
[0027] A method for preparing a low-sensitivity ovalbumin peptide, comprising the steps of:
[0028] (1) Pretreatment: prepare food-grade hydrogen peroxide with a mass fraction of solute of 0.8%, according to the mass ratio ovalbumin: food-grade hydrogen peroxide: potassium citrate: calcium chloride = 10:0.2:0.10:0.02, the Add high-grade hydrogen peroxide into the ovalbumin, fully stir and mix, then add potassium citrate and calcium chloride to the mixture in turn to obtain mixture A;
[0029] (2) Glycosylation: Dissolve 40 parts of mixture A and 40 parts of glucose in deionized water in parts by mass, and mix evenly after dissolving. The quality of deionized water is 5 times the total mass of mixture A and glucose to be dissolved ; After mixing evenly, freeze-drying, and after freeze-drying, react for 3 hours at a relative humidity of 60% to 80% and a temperature of 50 to 70°C to obtain sample B;
[0030] (3) Enzymolysis: Add pepsin enzymolysis solution whose mass is 4 times...
Embodiment 3
[0035] A method for preparing a low-sensitivity ovalbumin peptide, comprising the steps of:
[0036] (1) Pretreatment: configure food-grade hydrogen peroxide with a mass fraction of solute of 1.5%, according to the mass ratio ovalbumin: food-grade hydrogen peroxide: potassium citrate: calcium chloride = 10:0.2:0.14:0.02, the food Add high-grade hydrogen peroxide into the ovalbumin, fully stir and mix, then add potassium citrate and calcium chloride to the mixture in turn to obtain mixture A;
[0037] (2) Glycosylation: Dissolve 50 parts of mixture A and 50 parts of glucose in deionized water in parts by mass, and mix evenly after dissolving. The quality of deionized water is 5 times the total mass of mixture A and glucose to be dissolved ; After mixing evenly, freeze-drying, and after freeze-drying, react for 4 hours at a relative humidity of 60% to 80% and a temperature of 50 to 70°C to obtain sample B;
[0038] (3) Enzymolysis: Add pepsin enzymolysis solution with a mass 4 ...
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